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Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi

This study was performed to investigate the effect of plasticizers on the properties of the waste cooking oil based polyurethane (PU) solid polymer electrolytes (SPE).The polyurethane was prepared via solution casting method. Polyethylene Glycol (PEG) and Ethylene carbonate (EC) was chosen as plasti...

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Main Author: Mhd Huzaizi, Rahmatina
Format: Student Project
Language:English
Published: 2016
Subjects:
Temperature
Electrolytes, electrolyte solutions
Online Access:https://ir.uitm.edu.my/id/eprint/83644/1/83644.PDF
https://ir.uitm.edu.my/id/eprint/83644/
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spelling my.uitm.ir.836442024-01-14T08:55:12Z https://ir.uitm.edu.my/id/eprint/83644/ Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi Mhd Huzaizi, Rahmatina Temperature Electrolytes, electrolyte solutions This study was performed to investigate the effect of plasticizers on the properties of the waste cooking oil based polyurethane (PU) solid polymer electrolytes (SPE).The polyurethane was prepared via solution casting method. Polyethylene Glycol (PEG) and Ethylene carbonate (EC) was chosen as plasticizers. The PU SPE films were characterized by using Fourier Transform Infrared (FTIR), Electrochemical Impendence Spectroscopy (ElS), Thermogravimetric analysis (TGA), Differential scanning Calorimetry (DSC) and X-ray Diffraction (XRD). The highest ionic conductivity of 8.40 x 10-8 Scm-1 was achieved with the addition of plasticizer ethylene carbonate (EC) at room temperature and thermally analysis showed by DSC is the lowest transition glass, Tg obtained at 106.0°C. TGA was analyzed that five type of thermal degradation had been obtained. These confirmed as the molecular structure of PU SPE films were investigate by FTIR and the presence of urethane linkage and disappearance of NCO in peak the FTIR spectrum showed that diisocyanate was completely reacted to form PU SPE. The XRD showed that the PU SPE EC was highly amorphous due to broad hump became broader and intensity decreased. These observations indicated the synthesized PU SPE film possessed favorable properties to act as a base material in polymer electrolytes. 2016 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/83644/1/83644.PDF Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi. (2016) [Student Project] <http://terminalib.uitm.edu.my/83644.pdf> (Unpublished)
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic Temperature
Electrolytes, electrolyte solutions
spellingShingle Temperature
Electrolytes, electrolyte solutions
Mhd Huzaizi, Rahmatina
Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi
description This study was performed to investigate the effect of plasticizers on the properties of the waste cooking oil based polyurethane (PU) solid polymer electrolytes (SPE).The polyurethane was prepared via solution casting method. Polyethylene Glycol (PEG) and Ethylene carbonate (EC) was chosen as plasticizers. The PU SPE films were characterized by using Fourier Transform Infrared (FTIR), Electrochemical Impendence Spectroscopy (ElS), Thermogravimetric analysis (TGA), Differential scanning Calorimetry (DSC) and X-ray Diffraction (XRD). The highest ionic conductivity of 8.40 x 10-8 Scm-1 was achieved with the addition of plasticizer ethylene carbonate (EC) at room temperature and thermally analysis showed by DSC is the lowest transition glass, Tg obtained at 106.0°C. TGA was analyzed that five type of thermal degradation had been obtained. These confirmed as the molecular structure of PU SPE films were investigate by FTIR and the presence of urethane linkage and disappearance of NCO in peak the FTIR spectrum showed that diisocyanate was completely reacted to form PU SPE. The XRD showed that the PU SPE EC was highly amorphous due to broad hump became broader and intensity decreased. These observations indicated the synthesized PU SPE film possessed favorable properties to act as a base material in polymer electrolytes.
format Student Project
author Mhd Huzaizi, Rahmatina
author_facet Mhd Huzaizi, Rahmatina
author_sort Mhd Huzaizi, Rahmatina
title Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi
title_short Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi
title_full Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi
title_fullStr Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi
title_full_unstemmed Synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / Rahmatina Mhd Huzaizi
title_sort synthesis of waste cooking oil based polyurethane solid polymer electrolytes: the effect of plasticizers / rahmatina mhd huzaizi
publishDate 2016
url https://ir.uitm.edu.my/id/eprint/83644/1/83644.PDF
https://ir.uitm.edu.my/id/eprint/83644/
_version_ 1789429208486772736
score 13.211869

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