Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak
Synthesis of new hybrid nanocomposite material zinc-aluminium-9-hydroxy-9- fluorenecarboxylate was successfully accomplished by self assembly method with molar ratio of Zn to Al ; R= 2 at various concentration of 9-hydroxy-9-fluorenecarboxylate ranging from 0.2 M to 0.8 M . The pH of the synthesi...
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Faculty of Applied Sciences
2009
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| Online Access: | http://ir.uitm.edu.my/id/eprint/756/1/PPb_MOHD%20HAFIZ%20ABDUL%20RAZAK%20AS%2009_5.pdf http://ir.uitm.edu.my/id/eprint/756/ |
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my.uitm.ir.7562017-04-21T06:11:46Z http://ir.uitm.edu.my/id/eprint/756/ Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak Abdul Razak, Mohd Hafiz Synthesis of new hybrid nanocomposite material zinc-aluminium-9-hydroxy-9- fluorenecarboxylate was successfully accomplished by self assembly method with molar ratio of Zn to Al ; R= 2 at various concentration of 9-hydroxy-9-fluorenecarboxylate ranging from 0.2 M to 0.8 M . The pH of the synthesis was kept constant at 7.5. As a result of the successful intercalation of 9-hydroxy-9-fluorenecarboxylate anion into zincaluminium- layered double hydroxide, an expansion of the interlayer spacing from 8.9 Å in the layered double hydroxide to 14.3 Å in the zinc-aluminium9-hydroxy-9- fluorenecarboxylate nanocomposite could be observed in the PXRD diffractogram. The percentage loading of the guest anion, 9-hydroxy-9-fluorenecarboxylate in the layered double hydroxide was estimated to be about 76-78% (w/w) at the optimum condition Faculty of Applied Sciences 2009 Student Project NonPeerReviewed text en http://ir.uitm.edu.my/id/eprint/756/1/PPb_MOHD%20HAFIZ%20ABDUL%20RAZAK%20AS%2009_5.pdf Abdul Razak, Mohd Hafiz (2009) Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak. [Student Project] (Unpublished) |
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| description |
Synthesis of new hybrid nanocomposite material zinc-aluminium-9-hydroxy-9-
fluorenecarboxylate was successfully accomplished by self assembly method with molar
ratio of Zn to Al ; R= 2 at various concentration of 9-hydroxy-9-fluorenecarboxylate
ranging from 0.2 M to 0.8 M . The pH of the synthesis was kept constant at 7.5. As a
result of the successful intercalation of 9-hydroxy-9-fluorenecarboxylate anion into zincaluminium-
layered double hydroxide, an expansion of the interlayer spacing from 8.9 Å
in the layered double hydroxide to 14.3 Å in the zinc-aluminium9-hydroxy-9-
fluorenecarboxylate nanocomposite could be observed in the PXRD diffractogram. The
percentage loading of the guest anion, 9-hydroxy-9-fluorenecarboxylate in the layered
double hydroxide was estimated to be about 76-78% (w/w) at the optimum condition |
| format |
Student Project |
| author |
Abdul Razak, Mohd Hafiz |
| spellingShingle |
Abdul Razak, Mohd Hafiz Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak |
| author_facet |
Abdul Razak, Mohd Hafiz |
| author_sort |
Abdul Razak, Mohd Hafiz |
| title |
Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak |
| title_short |
Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak |
| title_full |
Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak |
| title_fullStr |
Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak |
| title_full_unstemmed |
Synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / Mohd Hafiz Abdul Razak |
| title_sort |
synthesis of organic-inorganic hybrid nanocomposite material 9-hydroxy-9 fluorenecarboxylic acid intercalated into zinc-aluminium layered double hydroxide / mohd hafiz abdul razak |
| publisher |
Faculty of Applied Sciences |
| publishDate |
2009 |
| url |
http://ir.uitm.edu.my/id/eprint/756/1/PPb_MOHD%20HAFIZ%20ABDUL%20RAZAK%20AS%2009_5.pdf http://ir.uitm.edu.my/id/eprint/756/ |
| _version_ |
1685648088390172672 |
| score |
13.211869 |