pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]

The influence of pH of the electrolyte used during anodization of Titanium substrate has been investigated in order to determine the optimum pH condition to form self-organized Titanium dioxide (TiO2) nanotubes (NTs) structure. The TiO2 NTs was formed by anodizing Titanium substrate in an electrolyt...

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Main Authors: Jani, Nur Aimi, Azizan, Izzatul Syifa, Razak, Nur Fatin, Mahat, Mohd Muzamir, Chiu, Weesiong, Abdul Rahman, Saadah
Format: Article
Language:English
Published: Faculty of AppliedSciences 2020
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Online Access:http://ir.uitm.edu.my/id/eprint/47046/1/47046.pdf
http://ir.uitm.edu.my/id/eprint/47046/
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spelling my.uitm.ir.470462021-06-07T13:53:10Z http://ir.uitm.edu.my/id/eprint/47046/ pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.] Jani, Nur Aimi Azizan, Izzatul Syifa Razak, Nur Fatin Mahat, Mohd Muzamir Chiu, Weesiong Abdul Rahman, Saadah Nanostructures Semiconductor physics The influence of pH of the electrolyte used during anodization of Titanium substrate has been investigated in order to determine the optimum pH condition to form self-organized Titanium dioxide (TiO2) nanotubes (NTs) structure. The TiO2 NTs was formed by anodizing Titanium substrate in an electrolyte containing 1M of sodium sulfate (Na2SO4) with 0.7 g of ammonium fluoride (NH4F) for 180 minutes with potential 20 V. The optimum conditions were determined by characterization using FESEM and XRD analysis. As shown in the result, it can be summarized that pH of the anodization electrolyte can affect the length and diameter of the NTs as confirmed by FESEM images. FESEM result shows that, the length of nanotubes increased as the pH increased which are from 50 nm to 424 nm for pH 5 and pH 7, respectively. However, at higher pH more than 7, the nanotube structure was collapsed and only form bulk oxide film. The FESEM result also supported by the XRD result as the peak at 24° increased up from pH 3 to pH 7 and drop at pH 9. Faculty of AppliedSciences 2020 Article PeerReviewed text en http://ir.uitm.edu.my/id/eprint/47046/1/47046.pdf ID47046 Jani, Nur Aimi and Azizan, Izzatul Syifa and Razak, Nur Fatin and Mahat, Mohd Muzamir and Chiu, Weesiong and Abdul Rahman, Saadah (2020) pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]. Science Letters (ScL), 14 (1). pp. 1-6. ISSN (eISSN) 2682-8626
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic Nanostructures
Semiconductor physics
spellingShingle Nanostructures
Semiconductor physics
Jani, Nur Aimi
Azizan, Izzatul Syifa
Razak, Nur Fatin
Mahat, Mohd Muzamir
Chiu, Weesiong
Abdul Rahman, Saadah
pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]
description The influence of pH of the electrolyte used during anodization of Titanium substrate has been investigated in order to determine the optimum pH condition to form self-organized Titanium dioxide (TiO2) nanotubes (NTs) structure. The TiO2 NTs was formed by anodizing Titanium substrate in an electrolyte containing 1M of sodium sulfate (Na2SO4) with 0.7 g of ammonium fluoride (NH4F) for 180 minutes with potential 20 V. The optimum conditions were determined by characterization using FESEM and XRD analysis. As shown in the result, it can be summarized that pH of the anodization electrolyte can affect the length and diameter of the NTs as confirmed by FESEM images. FESEM result shows that, the length of nanotubes increased as the pH increased which are from 50 nm to 424 nm for pH 5 and pH 7, respectively. However, at higher pH more than 7, the nanotube structure was collapsed and only form bulk oxide film. The FESEM result also supported by the XRD result as the peak at 24° increased up from pH 3 to pH 7 and drop at pH 9.
format Article
author Jani, Nur Aimi
Azizan, Izzatul Syifa
Razak, Nur Fatin
Mahat, Mohd Muzamir
Chiu, Weesiong
Abdul Rahman, Saadah
author_facet Jani, Nur Aimi
Azizan, Izzatul Syifa
Razak, Nur Fatin
Mahat, Mohd Muzamir
Chiu, Weesiong
Abdul Rahman, Saadah
author_sort Jani, Nur Aimi
title pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]
title_short pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]
title_full pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]
title_fullStr pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]
title_full_unstemmed pH Condition Influence Nanotube Structure of TiO2 by Anodizing Titanium Substrate / Nur Aimi Jani… [et al.]
title_sort ph condition influence nanotube structure of tio2 by anodizing titanium substrate / nur aimi jani… [et al.]
publisher Faculty of AppliedSciences
publishDate 2020
url http://ir.uitm.edu.my/id/eprint/47046/1/47046.pdf
http://ir.uitm.edu.my/id/eprint/47046/
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