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The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin

Waste citrus peels can be used as source of several bioactive compounds. Among these, limonene is the major constituent from citrus peels and is of great interest in several fields. In this study, the analysis of volatile compounds in four citrus peel samples, specifically limonene, was carried out...

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Main Author: Zainal Abidin, Nur Husna
Format: Student Project
Language:English
Published: 2015
Subjects:
Electrochemical analysis
Extraction (Chemistry)
Online Access:https://ir.uitm.edu.my/id/eprint/45646/1/45646.pdf
https://ir.uitm.edu.my/id/eprint/45646/
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spelling my.uitm.ir.456462022-12-14T03:38:40Z https://ir.uitm.edu.my/id/eprint/45646/ The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin Zainal Abidin, Nur Husna Electrochemical analysis Extraction (Chemistry) Waste citrus peels can be used as source of several bioactive compounds. Among these, limonene is the major constituent from citrus peels and is of great interest in several fields. In this study, the analysis of volatile compounds in four citrus peel samples, specifically limonene, was carried out using headspace solid - phase microextraction and gas chromatography - mass spectrometry detector to detect and relatively quantify the amount of limonene in all of the citrus peel samples. The conditions of SPME were optimized. The optimized extraction temperature, extraction time and desorption time were 70 °C, 40 min and 100 sec respectively. The retention time (tR.) for limonene in this study was 11.70 min. It was found that limonene was detected in all four citrus peel samples. Kaffir lime peel has the highest peak area of limonene which was 8.23 x 109 while key lime peel has the lowest peak area of limonene which was 3.24 x 109. 2015 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/45646/1/45646.pdf The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin. (2015) [Student Project] (Unpublished)
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic Electrochemical analysis
Extraction (Chemistry)
spellingShingle Electrochemical analysis
Extraction (Chemistry)
Zainal Abidin, Nur Husna
The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin
description Waste citrus peels can be used as source of several bioactive compounds. Among these, limonene is the major constituent from citrus peels and is of great interest in several fields. In this study, the analysis of volatile compounds in four citrus peel samples, specifically limonene, was carried out using headspace solid - phase microextraction and gas chromatography - mass spectrometry detector to detect and relatively quantify the amount of limonene in all of the citrus peel samples. The conditions of SPME were optimized. The optimized extraction temperature, extraction time and desorption time were 70 °C, 40 min and 100 sec respectively. The retention time (tR.) for limonene in this study was 11.70 min. It was found that limonene was detected in all four citrus peel samples. Kaffir lime peel has the highest peak area of limonene which was 8.23 x 109 while key lime peel has the lowest peak area of limonene which was 3.24 x 109.
format Student Project
author Zainal Abidin, Nur Husna
author_facet Zainal Abidin, Nur Husna
author_sort Zainal Abidin, Nur Husna
title The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin
title_short The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin
title_full The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin
title_fullStr The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin
title_full_unstemmed The extraction and detection of limonene (4-Isoprophenyl-L-Methyl Cyclohexene) from citrus peel using headspace solid phase micro-extraction (HS - SPME) and gas chromatography with mass spectrometry (GC-MS) / Nur Husna Zainal Abidin
title_sort extraction and detection of limonene (4-isoprophenyl-l-methyl cyclohexene) from citrus peel using headspace solid phase micro-extraction (hs - spme) and gas chromatography with mass spectrometry (gc-ms) / nur husna zainal abidin
publishDate 2015
url https://ir.uitm.edu.my/id/eprint/45646/1/45646.pdf
https://ir.uitm.edu.my/id/eprint/45646/
_version_ 1753791858156240896
score 13.211869

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