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Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah

Polyaniline powder was prepared by chemically synthesized of aniline monomer in dopant hydrochloric acid solution. The ammonium persulphate solution which was acted as oxidant was added in slowly in the reaction mixture by using magnetic stirrer at room temperature. The reaction took placed for 2h t...

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Main Author: Ilyah, Nurul Hidayah
Format: Student Project
Language:English
Published: 2009
Subjects:
Analytical chemistry
Plastics
Online Access:https://ir.uitm.edu.my/id/eprint/106622/1/106622.pdf
https://ir.uitm.edu.my/id/eprint/106622/
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spelling my.uitm.ir.1066222024-12-03T08:38:46Z https://ir.uitm.edu.my/id/eprint/106622/ Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah Ilyah, Nurul Hidayah Analytical chemistry Plastics Polyaniline powder was prepared by chemically synthesized of aniline monomer in dopant hydrochloric acid solution. The ammonium persulphate solution which was acted as oxidant was added in slowly in the reaction mixture by using magnetic stirrer at room temperature. The reaction took placed for 2h to complete the reaction. After 24h left, the dark green mixture was filtered and washed thoroughly with perchloric acid and disttiled water. The resulting polymer then was dried under vacuum at 80 °C for 4h. The powder then was characterized by FTIR, TGA, DSC and FESEM. Otherwise, the powder was dissolved in dimethyl sulfoxide and mixed with cellulose triacetate solution in dicholoromethane for making composite film. The film was also been characterized and its electrical conductivity was measured by using impedance spectroscopy. 2009 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/106622/1/106622.pdf Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah. (2009) [Student Project] <http://terminalib.uitm.edu.my/106622.pdf> (Unpublished)
institution Universiti Teknologi Mara
building Tun Abdul Razak Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
url_provider http://ir.uitm.edu.my/
language English
topic Analytical chemistry
Plastics
spellingShingle Analytical chemistry
Plastics
Ilyah, Nurul Hidayah
Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah
description Polyaniline powder was prepared by chemically synthesized of aniline monomer in dopant hydrochloric acid solution. The ammonium persulphate solution which was acted as oxidant was added in slowly in the reaction mixture by using magnetic stirrer at room temperature. The reaction took placed for 2h to complete the reaction. After 24h left, the dark green mixture was filtered and washed thoroughly with perchloric acid and disttiled water. The resulting polymer then was dried under vacuum at 80 °C for 4h. The powder then was characterized by FTIR, TGA, DSC and FESEM. Otherwise, the powder was dissolved in dimethyl sulfoxide and mixed with cellulose triacetate solution in dicholoromethane for making composite film. The film was also been characterized and its electrical conductivity was measured by using impedance spectroscopy.
format Student Project
author Ilyah, Nurul Hidayah
author_facet Ilyah, Nurul Hidayah
author_sort Ilyah, Nurul Hidayah
title Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah
title_short Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah
title_full Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah
title_fullStr Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah
title_full_unstemmed Chemical synthesis and characterization of polyaniline / Nurul Hidayah Ilyah
title_sort chemical synthesis and characterization of polyaniline / nurul hidayah ilyah
publishDate 2009
url https://ir.uitm.edu.my/id/eprint/106622/1/106622.pdf
https://ir.uitm.edu.my/id/eprint/106622/
_version_ 1817847363199303680
score 13.244413

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