Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles

Nano-scale powder of Magnesium (Mg) is found to play the dual role of catalyst and precursor with Boron-10 (10B) in the synthesis of Magnesium diboride nanoparticles (Mg10B2NPs) at 800 °C. Catalytically, Mg softens and melts enriched Boron at a relatively lower temperature than its actual boiling po...

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Main Authors: Ahmad, P., Khandaker, Mayeen Uddin *, Jamil, S., Rehman, F., Muhammad, N., Ullah, Z., Rauf Khan, M., Khan, G., Alotaibi, M. A., Alharthi, A. I., Din, I. U., Hussain, F., Khan, M. I., Ali, H.
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Published: Elsevier 2020
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Online Access:http://eprints.sunway.edu.my/1607/
http://doi.org/10.1016/j.ceramint.2020.07.156
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spelling my.sunway.eprints.16072021-03-11T07:16:43Z http://eprints.sunway.edu.my/1607/ Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles Ahmad, P. Khandaker, Mayeen Uddin * Jamil, S. Rehman, F. Muhammad, N. Ullah, Z. Rauf Khan, M. Khan, G. Alotaibi, M. A. Alharthi, A. I. Din, I. U. Hussain, F. Khan, M. I. Ali, H. R895-920 Medical Physics/Medical Radiology Nano-scale powder of Magnesium (Mg) is found to play the dual role of catalyst and precursor with Boron-10 (10B) in the synthesis of Magnesium diboride nanoparticles (Mg10B2NPs) at 800 °C. Catalytically, Mg softens and melts enriched Boron at a relatively lower temperature than its actual boiling point. As a precursor, it reacts with enriched Boron and forms the Mg10B2 compound. The nano-size catalyst and precursors help to grow the as-formed Mg10B2 compound in the form of nanoparticles. The shape or morphology of the synthesized Mg10B2NPs is revealed via field emission scanning electron microscopy (FESEM). Energy dispersive x-ray (EDX) spectroscopy has been performed to spot the elemental composition, whereas, X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS) are used to verify the composition and study the phase of the synthesized particles. Elsevier 2020-12 Article PeerReviewed Ahmad, P. and Khandaker, Mayeen Uddin * and Jamil, S. and Rehman, F. and Muhammad, N. and Ullah, Z. and Rauf Khan, M. and Khan, G. and Alotaibi, M. A. and Alharthi, A. I. and Din, I. U. and Hussain, F. and Khan, M. I. and Ali, H. (2020) Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles. Ceramics International, 46 (17). pp. 26809-26812. ISSN 0272-8842 http://doi.org/10.1016/j.ceramint.2020.07.156 doi:10.1016/j.ceramint.2020.07.156
institution Sunway University
building Sunway Campus Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Sunway University
content_source Sunway Institutional Repository
url_provider http://eprints.sunway.edu.my/
topic R895-920 Medical Physics/Medical Radiology
spellingShingle R895-920 Medical Physics/Medical Radiology
Ahmad, P.
Khandaker, Mayeen Uddin *
Jamil, S.
Rehman, F.
Muhammad, N.
Ullah, Z.
Rauf Khan, M.
Khan, G.
Alotaibi, M. A.
Alharthi, A. I.
Din, I. U.
Hussain, F.
Khan, M. I.
Ali, H.
Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
description Nano-scale powder of Magnesium (Mg) is found to play the dual role of catalyst and precursor with Boron-10 (10B) in the synthesis of Magnesium diboride nanoparticles (Mg10B2NPs) at 800 °C. Catalytically, Mg softens and melts enriched Boron at a relatively lower temperature than its actual boiling point. As a precursor, it reacts with enriched Boron and forms the Mg10B2 compound. The nano-size catalyst and precursors help to grow the as-formed Mg10B2 compound in the form of nanoparticles. The shape or morphology of the synthesized Mg10B2NPs is revealed via field emission scanning electron microscopy (FESEM). Energy dispersive x-ray (EDX) spectroscopy has been performed to spot the elemental composition, whereas, X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS) are used to verify the composition and study the phase of the synthesized particles.
format Article
author Ahmad, P.
Khandaker, Mayeen Uddin *
Jamil, S.
Rehman, F.
Muhammad, N.
Ullah, Z.
Rauf Khan, M.
Khan, G.
Alotaibi, M. A.
Alharthi, A. I.
Din, I. U.
Hussain, F.
Khan, M. I.
Ali, H.
author_facet Ahmad, P.
Khandaker, Mayeen Uddin *
Jamil, S.
Rehman, F.
Muhammad, N.
Ullah, Z.
Rauf Khan, M.
Khan, G.
Alotaibi, M. A.
Alharthi, A. I.
Din, I. U.
Hussain, F.
Khan, M. I.
Ali, H.
author_sort Ahmad, P.
title Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_short Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_full Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_fullStr Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_full_unstemmed Dual role of Magnesium as a catalyst and precursor with enriched boron in the synthesis of Magnesium diboride nanoparticles
title_sort dual role of magnesium as a catalyst and precursor with enriched boron in the synthesis of magnesium diboride nanoparticles
publisher Elsevier
publishDate 2020
url http://eprints.sunway.edu.my/1607/
http://doi.org/10.1016/j.ceramint.2020.07.156
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score 13.211869