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Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles

The Fe3O4 magnetic nanoparticles (MNPs) attached with S-quinolin-2-yl-methyl-dithiocarbazate (SQ2MDTC) have been developed, aiming to function as the heavy metal adsorbent. The surface of MNPs was first coated with (3- aminopropyl)triethoxysilane (APTES) as cross-linker and then SQ2MDTC was covale...

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Main Authors: Abdul Rahman, Ahmad Jazmi, Miskam, Mazidatulakmam Akmam, How, Fiona Ni Foong
Format: Conference or Workshop Item
Language:English
Published: 2018
Subjects:
QD Chemistry
Online Access:http://irep.iium.edu.my/68775/1/selection%20%281%29.pdf
http://irep.iium.edu.my/68775/
http://www.iium.edu.my/skam31/
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spelling my.iium.irep.687752019-01-04T03:31:21Z http://irep.iium.edu.my/68775/ Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles Abdul Rahman, Ahmad Jazmi Miskam, Mazidatulakmam Akmam How, Fiona Ni Foong QD Chemistry The Fe3O4 magnetic nanoparticles (MNPs) attached with S-quinolin-2-yl-methyl-dithiocarbazate (SQ2MDTC) have been developed, aiming to function as the heavy metal adsorbent. The surface of MNPs was first coated with (3- aminopropyl)triethoxysilane (APTES) as cross-linker and then SQ2MDTC was covalently incorporated to the coated MNPs. The structural and surface characteristics were investigated by Fourier transform infrared spectroscopy (FT-IR), CHNS elemental analysis, thermogravimetric analysis (TGA), x-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and Brunauer-Emmett-Teller (BET) analysis. The SQ2MDTC functionalized MNPs exhibited high adsorption affinity for aqueous Cu(II) and Pb(II) ions when analysed using inductively coupled plasma optical emission spectrometer (ICP-OES), resulting from complexation of the metal ions by surface amino groups. Findings of the present work highlighted the potential of MNPSQ2MDTC as an effective adsorbent for the removal of heavy metal ions in water and wastewater treatment. 2018-08-17 Conference or Workshop Item PeerReviewed application/pdf en http://irep.iium.edu.my/68775/1/selection%20%281%29.pdf Abdul Rahman, Ahmad Jazmi and Miskam, Mazidatulakmam Akmam and How, Fiona Ni Foong (2018) Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles. In: International Conference of Analytical Sciences 2018 (SKAM 31), 17th-19th August 2018, Kuantan, Pahang. (Unpublished) http://www.iium.edu.my/skam31/
institution Universiti Islam Antarabangsa Malaysia
building IIUM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider International Islamic University Malaysia
content_source IIUM Repository (IREP)
url_provider http://irep.iium.edu.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Abdul Rahman, Ahmad Jazmi
Miskam, Mazidatulakmam Akmam
How, Fiona Ni Foong
Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
description The Fe3O4 magnetic nanoparticles (MNPs) attached with S-quinolin-2-yl-methyl-dithiocarbazate (SQ2MDTC) have been developed, aiming to function as the heavy metal adsorbent. The surface of MNPs was first coated with (3- aminopropyl)triethoxysilane (APTES) as cross-linker and then SQ2MDTC was covalently incorporated to the coated MNPs. The structural and surface characteristics were investigated by Fourier transform infrared spectroscopy (FT-IR), CHNS elemental analysis, thermogravimetric analysis (TGA), x-ray powder diffraction (XRD), field emission scanning electron microscopy (FESEM), and Brunauer-Emmett-Teller (BET) analysis. The SQ2MDTC functionalized MNPs exhibited high adsorption affinity for aqueous Cu(II) and Pb(II) ions when analysed using inductively coupled plasma optical emission spectrometer (ICP-OES), resulting from complexation of the metal ions by surface amino groups. Findings of the present work highlighted the potential of MNPSQ2MDTC as an effective adsorbent for the removal of heavy metal ions in water and wastewater treatment.
format Conference or Workshop Item
author Abdul Rahman, Ahmad Jazmi
Miskam, Mazidatulakmam Akmam
How, Fiona Ni Foong
author_facet Abdul Rahman, Ahmad Jazmi
Miskam, Mazidatulakmam Akmam
How, Fiona Ni Foong
author_sort Abdul Rahman, Ahmad Jazmi
title Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_short Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_full Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_fullStr Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_full_unstemmed Preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
title_sort preparation and characterization of s-quinolin-2-ylmethyldithiocarbazate functionalized magnetic nanoparticles
publishDate 2018
url http://irep.iium.edu.my/68775/1/selection%20%281%29.pdf
http://irep.iium.edu.my/68775/
http://www.iium.edu.my/skam31/
_version_ 1643618649876987904
score 13.211869

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