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Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst

Glycerol is the main by-product of biodiesel production that produces from transesterification process. In this research, focused was on hydrogen production via glycerol steam reforming using nickel loaded HZSM-5 catalyst. The catalysts were prepared by using different loading amount of nickel (0.5,...

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Main Authors: Azaman, Fazureen, Juahir, Hafizan, Mohamed, Mahadhir, Azid, Azman, Yunus, Kamaruzzaman, Abdul Rahman, Anis Farhana, Wan Ranizang, Wan Nur Anis Amira, Md Sanin, Fara Aiza, Amran, Mohammad Azizi, Zainal Abidin, Mohd Zaid Arqam, Hairoma, Norsyuhada, Sulaiman, Nur Hishaam, Zainal Abidin, Ismail
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia (UKM) 2015
Subjects:
QD Chemistry
Online Access:http://irep.iium.edu.my/45424/1/Hydrogen_gas_production_from_glycerol_via.pdf
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spelling my.iium.irep.454242017-08-09T07:14:55Z http://irep.iium.edu.my/45424/ Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst Azaman, Fazureen Juahir, Hafizan Mohamed, Mahadhir Azid, Azman Yunus, Kamaruzzaman Abdul Rahman, Anis Farhana Wan Ranizang, Wan Nur Anis Amira Md Sanin, Fara Aiza Amran, Mohammad Azizi Zainal Abidin, Mohd Zaid Arqam Hairoma, Norsyuhada Sulaiman, Nur Hishaam Zainal Abidin, Ismail QD Chemistry Glycerol is the main by-product of biodiesel production that produces from transesterification process. In this research, focused was on hydrogen production via glycerol steam reforming using nickel loaded HZSM-5 catalyst. The catalysts were prepared by using different loading amount of nickel (0.5, 1.0, 5.0, 10.0 and 15 wt %) on HZSM-5 catalyst through the wet impregnation method at temperature 500 ºC and atmospheric pressure. The catalyst was characterized by using XRD, FTIR and SEM. Then, only 15 wt % Ni loading has been chosen based on the parameter which is different range of catalyst weight (0.3-0.5g) at different range of glycerol flow rate (0.2-0.4mL/min) at temperature 600 ºC and atmospheric pressure. The products were analyzed by using gas-chromatography with thermal conductivity detector (GC-TCD) where it is used to identify the yield of hydrogen. The data of the experiment were analyzed by using Response Surface Methodology (RSM) in order to study the relationship of catalyst weight and glycerol flow rate. The results showed that the optimum condition to produce a maximum hydrogen yield with 15wt% Ni/HZSM-5 catalyst was 78.10004% at glycerol flow rate of 0.356484 mL/min and catalyst weight of 0.429267 g. Universiti Kebangsaan Malaysia (UKM) 2015 Article REM application/pdf en http://irep.iium.edu.my/45424/1/Hydrogen_gas_production_from_glycerol_via.pdf Azaman, Fazureen and Juahir, Hafizan and Mohamed, Mahadhir and Azid, Azman and Yunus, Kamaruzzaman and Abdul Rahman, Anis Farhana and Wan Ranizang, Wan Nur Anis Amira and Md Sanin, Fara Aiza and Amran, Mohammad Azizi and Zainal Abidin, Mohd Zaid Arqam and Hairoma, Norsyuhada and Sulaiman, Nur Hishaam and Zainal Abidin, Ismail (2015) Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst. Malaysian Journal of Analytical Sciences (MJAS), 19 (5). pp. 1043-1055. ISSN 1394-2506 http://www.ukm.my/mjas/About%20MJAS.html
institution Universiti Islam Antarabangsa Malaysia
building IIUM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider International Islamic University Malaysia
content_source IIUM Repository (IREP)
url_provider http://irep.iium.edu.my/
language English
topic QD Chemistry
spellingShingle QD Chemistry
Azaman, Fazureen
Juahir, Hafizan
Mohamed, Mahadhir
Azid, Azman
Yunus, Kamaruzzaman
Abdul Rahman, Anis Farhana
Wan Ranizang, Wan Nur Anis Amira
Md Sanin, Fara Aiza
Amran, Mohammad Azizi
Zainal Abidin, Mohd Zaid Arqam
Hairoma, Norsyuhada
Sulaiman, Nur Hishaam
Zainal Abidin, Ismail
Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
description Glycerol is the main by-product of biodiesel production that produces from transesterification process. In this research, focused was on hydrogen production via glycerol steam reforming using nickel loaded HZSM-5 catalyst. The catalysts were prepared by using different loading amount of nickel (0.5, 1.0, 5.0, 10.0 and 15 wt %) on HZSM-5 catalyst through the wet impregnation method at temperature 500 ºC and atmospheric pressure. The catalyst was characterized by using XRD, FTIR and SEM. Then, only 15 wt % Ni loading has been chosen based on the parameter which is different range of catalyst weight (0.3-0.5g) at different range of glycerol flow rate (0.2-0.4mL/min) at temperature 600 ºC and atmospheric pressure. The products were analyzed by using gas-chromatography with thermal conductivity detector (GC-TCD) where it is used to identify the yield of hydrogen. The data of the experiment were analyzed by using Response Surface Methodology (RSM) in order to study the relationship of catalyst weight and glycerol flow rate. The results showed that the optimum condition to produce a maximum hydrogen yield with 15wt% Ni/HZSM-5 catalyst was 78.10004% at glycerol flow rate of 0.356484 mL/min and catalyst weight of 0.429267 g.
format Article
author Azaman, Fazureen
Juahir, Hafizan
Mohamed, Mahadhir
Azid, Azman
Yunus, Kamaruzzaman
Abdul Rahman, Anis Farhana
Wan Ranizang, Wan Nur Anis Amira
Md Sanin, Fara Aiza
Amran, Mohammad Azizi
Zainal Abidin, Mohd Zaid Arqam
Hairoma, Norsyuhada
Sulaiman, Nur Hishaam
Zainal Abidin, Ismail
author_facet Azaman, Fazureen
Juahir, Hafizan
Mohamed, Mahadhir
Azid, Azman
Yunus, Kamaruzzaman
Abdul Rahman, Anis Farhana
Wan Ranizang, Wan Nur Anis Amira
Md Sanin, Fara Aiza
Amran, Mohammad Azizi
Zainal Abidin, Mohd Zaid Arqam
Hairoma, Norsyuhada
Sulaiman, Nur Hishaam
Zainal Abidin, Ismail
author_sort Azaman, Fazureen
title Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
title_short Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
title_full Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
title_fullStr Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
title_full_unstemmed Hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
title_sort hydrogen gas production from glycerol via steam reforming using nickel loaded zeolite catalyst
publisher Universiti Kebangsaan Malaysia (UKM)
publishDate 2015
url http://irep.iium.edu.my/45424/1/Hydrogen_gas_production_from_glycerol_via.pdf
http://irep.iium.edu.my/45424/
http://www.ukm.my/mjas/About%20MJAS.html
_version_ 1643612784033792000
score 13.211869

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