Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study

Triphasic calcium phosphate, composed of a more stable phase hydroxyapatite (HA) and highly soluble tricalcium phosphates (α- and β-TCP) has been synthesized through hydrothermal method. In the present work, an in-situ method to disperse 1wt% multiwall carbon nanotubes (MWCNTs) within HA/TCP powder...

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Main Authors: Gunawan, Gunawan, Sopyan, Iis, Nurfaezah, Siti, Ammar, Mohd
Format: Article
Language:English
Published: Trans Tech Publications, Switzerland 2013
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Online Access:http://irep.iium.edu.my/28637/1/KEM_Triphasic_CaP_gnw_2013.pdf
http://irep.iium.edu.my/28637/
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spelling my.iium.irep.286372015-03-04T00:41:59Z http://irep.iium.edu.my/28637/ Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study Gunawan, Gunawan Sopyan, Iis Nurfaezah, Siti Ammar, Mohd TA401 Materials of engineering and construction TP785 Clay industries. Ceramics. Glass. Cement industries Triphasic calcium phosphate, composed of a more stable phase hydroxyapatite (HA) and highly soluble tricalcium phosphates (α- and β-TCP) has been synthesized through hydrothermal method. In the present work, an in-situ method to disperse 1wt% multiwall carbon nanotubes (MWCNTs) within HA/TCP powder has been used in order to develop HA/TCP-CNTs composite. XRD results confirmed the formation of HA, α-TCP and β-TCP in both as-prepared powder and composite samples. The graphite peaks appeared in the composite samples as well. FTIR analysis of sintered compacted powder showed the formation of weak bands of PO43- as the temperature was increased. The sintered compacts were mechanically tested by Vickers microhardness indentation method. HA/TCP-CNTs composite was found to have a significant of Vickers Hardness of 1.98 GPa after 1100oC sintering. The morphology analysis showed that in-situ deposition technique provides homogeneous dispersion of CNTs in the calcium phosphate matrix. Trans Tech Publications, Switzerland 2013 Article REM application/pdf en http://irep.iium.edu.my/28637/1/KEM_Triphasic_CaP_gnw_2013.pdf Gunawan, Gunawan and Sopyan, Iis and Nurfaezah, Siti and Ammar, Mohd (2013) Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study. Key Engineering Materials, 531-32. pp. 258-261. ISSN 1013-9826 10.4028/www.scientific.net/KEM.531-532.258
institution Universiti Islam Antarabangsa Malaysia
building IIUM Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider International Islamic University Malaysia
content_source IIUM Repository (IREP)
url_provider http://irep.iium.edu.my/
language English
topic TA401 Materials of engineering and construction
TP785 Clay industries. Ceramics. Glass. Cement industries
spellingShingle TA401 Materials of engineering and construction
TP785 Clay industries. Ceramics. Glass. Cement industries
Gunawan, Gunawan
Sopyan, Iis
Nurfaezah, Siti
Ammar, Mohd
Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study
description Triphasic calcium phosphate, composed of a more stable phase hydroxyapatite (HA) and highly soluble tricalcium phosphates (α- and β-TCP) has been synthesized through hydrothermal method. In the present work, an in-situ method to disperse 1wt% multiwall carbon nanotubes (MWCNTs) within HA/TCP powder has been used in order to develop HA/TCP-CNTs composite. XRD results confirmed the formation of HA, α-TCP and β-TCP in both as-prepared powder and composite samples. The graphite peaks appeared in the composite samples as well. FTIR analysis of sintered compacted powder showed the formation of weak bands of PO43- as the temperature was increased. The sintered compacts were mechanically tested by Vickers microhardness indentation method. HA/TCP-CNTs composite was found to have a significant of Vickers Hardness of 1.98 GPa after 1100oC sintering. The morphology analysis showed that in-situ deposition technique provides homogeneous dispersion of CNTs in the calcium phosphate matrix.
format Article
author Gunawan, Gunawan
Sopyan, Iis
Nurfaezah, Siti
Ammar, Mohd
author_facet Gunawan, Gunawan
Sopyan, Iis
Nurfaezah, Siti
Ammar, Mohd
author_sort Gunawan, Gunawan
title Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study
title_short Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study
title_full Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study
title_fullStr Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study
title_full_unstemmed Development of triphasic calcium phosphate–carbon nanotubes (HA/TCP-CNT) composite: a preliminary study
title_sort development of triphasic calcium phosphate–carbon nanotubes (ha/tcp-cnt) composite: a preliminary study
publisher Trans Tech Publications, Switzerland
publishDate 2013
url http://irep.iium.edu.my/28637/1/KEM_Triphasic_CaP_gnw_2013.pdf
http://irep.iium.edu.my/28637/
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score 13.211869