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Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time

This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180°C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis...

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Main Authors: Nik Roselina, N.R, Azizan, A, Lockman, Z
Format: Article
Language:English
Published: Universiti Kebangsaan Malaysia 2012
Online Access:http://journalarticle.ukm.my/5427/1/15%2520N.R%2520Nik%2520roselina.pdf
http://journalarticle.ukm.my/5427/
http://www.ukm.my/jsm/
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spelling my-ukm.journal.54272016-12-14T06:38:25Z http://journalarticle.ukm.my/5427/ Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time Nik Roselina, N.R Azizan, A Lockman, Z This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180°C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis also indicated that the as-synthesized nanoparticles were pure Ni with face-centered cubic (fcc) crystal structure. Transmission electron microscopy (TEM) results showed that the sample with heating duration of 15 min has the most narrow size distribution and the size increased as the reaction time increased. Universiti Kebangsaan Malaysia 2012-08 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/5427/1/15%2520N.R%2520Nik%2520roselina.pdf Nik Roselina, N.R and Azizan, A and Lockman, Z (2012) Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time. Sains Malaysiana, 41 (8). pp. 1037-1042. ISSN 0126-6039 http://www.ukm.my/jsm/
institution Universiti Kebangsaan Malaysia
building Perpustakaan Tun Sri Lanang Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Kebangsaan Malaysia
content_source UKM Journal Article Repository
url_provider http://journalarticle.ukm.my/
language English
description This paper presents facile and rapid synthesis route of Ni nanoparticles at approximately 180°C in the mixture composed of ethylene glycol (EG) with hydrazine (N2H4) as a reducing agent. X-ray diffraction (XRD) analysis revealed that Ni2+ can be reduced completely to Ni metal in 15 min. XRD analysis also indicated that the as-synthesized nanoparticles were pure Ni with face-centered cubic (fcc) crystal structure. Transmission electron microscopy (TEM) results showed that the sample with heating duration of 15 min has the most narrow size distribution and the size increased as the reaction time increased.
format Article
author Nik Roselina, N.R
Azizan, A
Lockman, Z
spellingShingle Nik Roselina, N.R
Azizan, A
Lockman, Z
Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
author_facet Nik Roselina, N.R
Azizan, A
Lockman, Z
author_sort Nik Roselina, N.R
title Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_short Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_full Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_fullStr Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_full_unstemmed Synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
title_sort synthesis of nickel nanoparticles via non-aqueous polyol method: effect of reaction time
publisher Universiti Kebangsaan Malaysia
publishDate 2012
url http://journalarticle.ukm.my/5427/1/15%2520N.R%2520Nik%2520roselina.pdf
http://journalarticle.ukm.my/5427/
http://www.ukm.my/jsm/
_version_ 1643736410271776768
score 13.211869

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