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Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test

In this present study, silver nanoparticles were synthesized by green biological synthesis method using plant extract from fruit peel of Citrus aurantifolia as reducing agents. All the parameters in the synthesis of silver nanoparticles (AgNPs) were optimized to achieve a better yield, controlled si...

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Main Authors: Nabila Adlina Nasruddin,, Nur Raihana Ithnin,, Hidayatulfathi Othman,, Zatul-’Iffah Abu Hasan,, Norashiqin Misni,
Format: Article
Language:English
Published: Penerbit Universiti Kebangsaan Malaysia 2024
Online Access:http://journalarticle.ukm.my/24038/1/SEE%2012.pdf
http://journalarticle.ukm.my/24038/
https://www.ukm.my/jsm/english_journals/vol53num5_2024/contentsVol53num5_2024.html
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spelling my-ukm.journal.240382024-08-19T03:51:51Z http://journalarticle.ukm.my/24038/ Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test Nabila Adlina Nasruddin, Nur Raihana Ithnin, Hidayatulfathi Othman, Zatul-’Iffah Abu Hasan, Norashiqin Misni, In this present study, silver nanoparticles were synthesized by green biological synthesis method using plant extract from fruit peel of Citrus aurantifolia as reducing agents. All the parameters in the synthesis of silver nanoparticles (AgNPs) were optimized to achieve a better yield, controlled size and stability of the particles. The biosynthesis of silver nanoparticles was monitored via UV-vis spectrophotometer and stability test was done. The resulting UV-Vis spectra of synthesized AgNPs from C. aurantifolia fruit peel extract (CAFPE) showed standard surface plasmon resonance band at 420 nm which indicated the presence of AgNPs. The optimum result was obtained with an optimum concentration at 4 mM AgNO3 , leaving in a dark room temperature for 24 h and using a concentration 1:3 ratio (extract: silver nitrate). Moreover, the stability of the CAFPE-AgNPs was also observed after 30 days of synthesis and even up to 10 months, indicating optimization plays major role towards the stability fate of nanoparticles. The FTIR analysis showed possible functional groups of biomolecules that play roles in the bioreduction and capping of silver nanoparticles. In addition, it is believed that these parameters are highly suitable for bulk production of single spherical AgNPs with diameter 29.6- 45.2 nm confirmed via FESEM. Thus, the obtained results clearly suggest that optimization of silver nanoparticles may have important role in attaining a better yield and stability of metal nanoparticles, refraining back to its original structure or particles. Penerbit Universiti Kebangsaan Malaysia 2024 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/24038/1/SEE%2012.pdf Nabila Adlina Nasruddin, and Nur Raihana Ithnin, and Hidayatulfathi Othman, and Zatul-’Iffah Abu Hasan, and Norashiqin Misni, (2024) Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test. Sains Malaysiana, 53 (5). pp. 1119-1131. ISSN 0126-6039 https://www.ukm.my/jsm/english_journals/vol53num5_2024/contentsVol53num5_2024.html
institution Universiti Kebangsaan Malaysia
building Tun Sri Lanang Library
collection Institutional Repository
continent Asia
country Malaysia
content_provider Universiti Kebangsaan Malaysia
content_source UKM Journal Article Repository
url_provider http://journalarticle.ukm.my/
language English
description In this present study, silver nanoparticles were synthesized by green biological synthesis method using plant extract from fruit peel of Citrus aurantifolia as reducing agents. All the parameters in the synthesis of silver nanoparticles (AgNPs) were optimized to achieve a better yield, controlled size and stability of the particles. The biosynthesis of silver nanoparticles was monitored via UV-vis spectrophotometer and stability test was done. The resulting UV-Vis spectra of synthesized AgNPs from C. aurantifolia fruit peel extract (CAFPE) showed standard surface plasmon resonance band at 420 nm which indicated the presence of AgNPs. The optimum result was obtained with an optimum concentration at 4 mM AgNO3 , leaving in a dark room temperature for 24 h and using a concentration 1:3 ratio (extract: silver nitrate). Moreover, the stability of the CAFPE-AgNPs was also observed after 30 days of synthesis and even up to 10 months, indicating optimization plays major role towards the stability fate of nanoparticles. The FTIR analysis showed possible functional groups of biomolecules that play roles in the bioreduction and capping of silver nanoparticles. In addition, it is believed that these parameters are highly suitable for bulk production of single spherical AgNPs with diameter 29.6- 45.2 nm confirmed via FESEM. Thus, the obtained results clearly suggest that optimization of silver nanoparticles may have important role in attaining a better yield and stability of metal nanoparticles, refraining back to its original structure or particles.
format Article
author Nabila Adlina Nasruddin,
Nur Raihana Ithnin,
Hidayatulfathi Othman,
Zatul-’Iffah Abu Hasan,
Norashiqin Misni,
spellingShingle Nabila Adlina Nasruddin,
Nur Raihana Ithnin,
Hidayatulfathi Othman,
Zatul-’Iffah Abu Hasan,
Norashiqin Misni,
Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
author_facet Nabila Adlina Nasruddin,
Nur Raihana Ithnin,
Hidayatulfathi Othman,
Zatul-’Iffah Abu Hasan,
Norashiqin Misni,
author_sort Nabila Adlina Nasruddin,
title Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
title_short Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
title_full Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
title_fullStr Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
title_full_unstemmed Green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
title_sort green synthesis of silver nanoparticles using aqueous fruit peel extract of citrus aurantifolia: optimization, its characterization and stability test
publisher Penerbit Universiti Kebangsaan Malaysia
publishDate 2024
url http://journalarticle.ukm.my/24038/1/SEE%2012.pdf
http://journalarticle.ukm.my/24038/
https://www.ukm.my/jsm/english_journals/vol53num5_2024/contentsVol53num5_2024.html
_version_ 1809139048949743616
score 13.211869

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