Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction
Bisphenol A (BPA) is a xenoestrogen that widely used in manufacture of plastics. Concern is mounting up when the application of BPA is widespread. A simple sample pre-treatment technique termed membrane-protected liquid phase microextraction (MP-LPME) combined with high performance liquid chromatogr...
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Penerbit Universiti Kebangsaan Malaysia
2020
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Online Access: | http://journalarticle.ukm.my/14730/1/ARTIKEL%206.pdf http://journalarticle.ukm.my/14730/ http://www.ukm.my/jsm/malay_journals/jilid49bil1_2020/KandunganJilid49Bil1_2020.html |
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my-ukm.journal.147302020-06-12T04:49:11Z http://journalarticle.ukm.my/14730/ Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction Loh, Thung Ying Wan Mohd Afiq Wan Mohd Khalik, Loh, Saw Hong Bisphenol A (BPA) is a xenoestrogen that widely used in manufacture of plastics. Concern is mounting up when the application of BPA is widespread. A simple sample pre-treatment technique termed membrane-protected liquid phase microextraction (MP-LPME) combined with high performance liquid chromatography (HPLC)-fluorescence detection (FD) was developed for the determination of BPA in beverages and environmental water samples. The MP-LPME technique utilized a nylon membrane to hold the extractant (1-octanol) and prevent the extractant from dissolution into sample solution during agitation. Under optimal extraction conditions, the MP-LPME-HPLC-FD demonstrated ultra-trace detection of BPA and insignificant matrix effect extraction with good relative recoveries in the range of 87.1-99.7% from spiked beverage and environmental water samples. The membrane can be re-applied in the MP-LPME after the first usage and offered relative recovery of > 94%. The MP-LPME technique is eco-friendly as it consumes only minute amounts of organic solvent which is supportive to green analysis. Penerbit Universiti Kebangsaan Malaysia 2020-01 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/14730/1/ARTIKEL%206.pdf Loh, Thung Ying and Wan Mohd Afiq Wan Mohd Khalik, and Loh, Saw Hong (2020) Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction. Sains Malaysiana, 49 (1). pp. 49-55. ISSN 0126-6039 http://www.ukm.my/jsm/malay_journals/jilid49bil1_2020/KandunganJilid49Bil1_2020.html |
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Bisphenol A (BPA) is a xenoestrogen that widely used in manufacture of plastics. Concern is mounting up when the application of BPA is widespread. A simple sample pre-treatment technique termed membrane-protected liquid phase microextraction (MP-LPME) combined with high performance liquid chromatography (HPLC)-fluorescence detection (FD) was developed for the determination of BPA in beverages and environmental water samples. The MP-LPME technique utilized a nylon membrane to hold the extractant (1-octanol) and prevent the extractant from dissolution into sample solution during agitation. Under optimal extraction conditions, the MP-LPME-HPLC-FD demonstrated ultra-trace detection of BPA and insignificant matrix effect extraction with good relative recoveries in the range of 87.1-99.7% from spiked beverage and environmental water samples. The membrane can be re-applied in the MP-LPME after the first usage and offered relative recovery of > 94%. The MP-LPME technique is eco-friendly as it consumes only minute amounts of organic solvent which is supportive to green analysis. |
format |
Article |
author |
Loh, Thung Ying Wan Mohd Afiq Wan Mohd Khalik, Loh, Saw Hong |
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Loh, Thung Ying Wan Mohd Afiq Wan Mohd Khalik, Loh, Saw Hong Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction |
author_facet |
Loh, Thung Ying Wan Mohd Afiq Wan Mohd Khalik, Loh, Saw Hong |
author_sort |
Loh, Thung Ying |
title |
Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction |
title_short |
Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction |
title_full |
Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction |
title_fullStr |
Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction |
title_full_unstemmed |
Simple extraction of bisphenol A in beverages and water by membrane-protected liquid phase microextraction |
title_sort |
simple extraction of bisphenol a in beverages and water by membrane-protected liquid phase microextraction |
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Penerbit Universiti Kebangsaan Malaysia |
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2020 |
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http://journalarticle.ukm.my/14730/1/ARTIKEL%206.pdf http://journalarticle.ukm.my/14730/ http://www.ukm.my/jsm/malay_journals/jilid49bil1_2020/KandunganJilid49Bil1_2020.html |
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