Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography
Poly(styrene-divinyl benzene) (PS-DVB) monoliths were synthesized by in-situ polymerization in a 2.1 mm × 150 mm high performance liquid chromatography, (HPLC) column. The physical properties ofthe monolith were studied by FTIR and SEM. IR spectra of the monolith confirmed the formation of PS-DVB w...
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| Format: | Monograph |
| Language: | en |
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SPS, UTM
2006
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| Online Access: | http://eprints.utm.my/1756/1/2006_paper_norsyariza_abd_aziz_for_RPCES.pdf http://eprints.utm.my/1756/ |
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| _version_ | 1845470535568326656 |
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| author | Abd. Aziz, Norsyariza Abu Naim, Ahmedy Sanagi, Mohd. Marsin Wan Ibrahim, Wan Aini |
| author_facet | Abd. Aziz, Norsyariza Abu Naim, Ahmedy Sanagi, Mohd. Marsin Wan Ibrahim, Wan Aini |
| author_sort | Abd. Aziz, Norsyariza |
| building | UTM Library |
| collection | Institutional Repository |
| content_provider | Universiti Teknologi Malaysia |
| content_source | UTM Institutional Repository |
| continent | Asia |
| country | Malaysia |
| description | Poly(styrene-divinyl benzene) (PS-DVB) monoliths were synthesized by in-situ polymerization in a 2.1 mm × 150 mm high performance liquid chromatography, (HPLC) column. The physical properties ofthe monolith were studied by FTIR and SEM. IR spectra of the monolith confirmed the formation of PS-DVB whereas SEM analysis shows that the PS-DVB monolith gave the cauliflower structure. The performance of the synthesized column was evaluated by HPLC and compared with commercial PS-DVB column. The separations were carried out using 4 test compounds; benzaldehyde, nitrobenzene,phenol and toluene. Although the monolith column was less efficient than commercial packed PS-DVB column, the monolith gives faster analysis time. |
| format | Monograph |
| id | my.utm.eprints-1756 |
| institution | Universiti Teknologi Malaysia |
| language | en |
| publishDate | 2006 |
| publisher | SPS, UTM |
| record_format | eprints |
| spelling | my.utm.eprints-17562017-10-08T08:05:17Z http://eprints.utm.my/1756/ Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography Abd. Aziz, Norsyariza Abu Naim, Ahmedy Sanagi, Mohd. Marsin Wan Ibrahim, Wan Aini QD Chemistry Poly(styrene-divinyl benzene) (PS-DVB) monoliths were synthesized by in-situ polymerization in a 2.1 mm × 150 mm high performance liquid chromatography, (HPLC) column. The physical properties ofthe monolith were studied by FTIR and SEM. IR spectra of the monolith confirmed the formation of PS-DVB whereas SEM analysis shows that the PS-DVB monolith gave the cauliflower structure. The performance of the synthesized column was evaluated by HPLC and compared with commercial PS-DVB column. The separations were carried out using 4 test compounds; benzaldehyde, nitrobenzene,phenol and toluene. Although the monolith column was less efficient than commercial packed PS-DVB column, the monolith gives faster analysis time. SPS, UTM 2006 Monograph NonPeerReviewed application/pdf en http://eprints.utm.my/1756/1/2006_paper_norsyariza_abd_aziz_for_RPCES.pdf Abd. Aziz, Norsyariza and Abu Naim, Ahmedy and Sanagi, Mohd. Marsin and Wan Ibrahim, Wan Aini (2006) Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography. Working Paper. SPS, UTM. (Unpublished) |
| spellingShingle | QD Chemistry Abd. Aziz, Norsyariza Abu Naim, Ahmedy Sanagi, Mohd. Marsin Wan Ibrahim, Wan Aini Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography |
| title | Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography
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| title_full | Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography
|
| title_fullStr | Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography
|
| title_full_unstemmed | Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography
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| title_short | Poly(Styrene-Divinyl Benzene)-Based Monolithic Column For High Performance Liquid Chromatography
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| title_sort | poly(styrene-divinyl benzene)-based monolithic column for high performance liquid chromatography |
| topic | QD Chemistry |
| url | http://eprints.utm.my/1756/1/2006_paper_norsyariza_abd_aziz_for_RPCES.pdf http://eprints.utm.my/1756/ |
| url_provider | http://eprints.utm.my/ |