Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method
Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine...
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| Format: | Conference or Workshop Item |
| Language: | en |
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2009
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| Online Access: | http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf http://eprints.utem.edu.my/id/eprint/9785/ |
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| _version_ | 1832716439263379456 |
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| author | Al-Amani, Umar |
| author_facet | Al-Amani, Umar |
| author_sort | Al-Amani, Umar |
| building | UTEM Library |
| collection | Institutional Repository |
| content_provider | Universiti Teknikal Malaysia Melaka |
| content_source | UTEM Institutional Repository |
| continent | Asia |
| country | Malaysia |
| description | Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4
and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the
phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine the
formation of Bi4Ti3O12. Pure Bi4Ti3O12 powder was successfully formed with Ti addition after calcination
at 800oC for 3 h. The average crystallite sizes produced were 77.9 nm, 63.6 nm and 51.8 nm with mol ratio
of 4:3.1, 4:3.4 and 4:3.6, respectively. The results obtained infer that the relative amount of Ti was
identified as limiting reagent in the combustion reaction and was also considered as key factor to achieve
single-phase Bi4Ti3O12 |
| format | Conference or Workshop Item |
| id | my.utem.eprints-9785 |
| institution | Universiti Teknikal Malaysia Melaka |
| language | en |
| publishDate | 2009 |
| record_format | eprints |
| spelling | my.utem.eprints-97852015-05-28T04:06:35Z http://eprints.utem.edu.my/id/eprint/9785/ Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method Al-Amani, Umar T Technology (General) Bi4Ti3O12was synthesized by fuel-free combustion method using Bi(NO3)3.5H2O and Ti[OCH (CH3)2]4 and subsequent calcination. The effect of processing parameters such as Bi addition and Ti addition on the phase formation of Bi4Ti3O12was investigated. X-Ray Diffraction analysis was used to determine the formation of Bi4Ti3O12. Pure Bi4Ti3O12 powder was successfully formed with Ti addition after calcination at 800oC for 3 h. The average crystallite sizes produced were 77.9 nm, 63.6 nm and 51.8 nm with mol ratio of 4:3.1, 4:3.4 and 4:3.6, respectively. The results obtained infer that the relative amount of Ti was identified as limiting reagent in the combustion reaction and was also considered as key factor to achieve single-phase Bi4Ti3O12 2009 Conference or Workshop Item PeerReviewed application/pdf en http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf Al-Amani, Umar (2009) Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method. In: 4th International Conference on Recent Advances in Materials, Minerals, Environment and 2nd Asian Symposium on materials and Processing (RAMM & ASMP), 1-3 Jun 2009, Bayview Beach Resort, Batu Ferringi, Penang, Malaysia. |
| spellingShingle | T Technology (General) Al-Amani, Umar Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method |
| title | Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method |
| title_full | Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method |
| title_fullStr | Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method |
| title_full_unstemmed | Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method |
| title_short | Effect of Bi and Ti additions on the phase formation of Bi4Ti3O12 using fuel-free combustion method |
| title_sort | effect of bi and ti additions on the phase formation of bi4ti3o12 using fuel-free combustion method |
| topic | T Technology (General) |
| url | http://eprints.utem.edu.my/id/eprint/9785/1/RRAMM_and_ASMP_2009.pdf http://eprints.utem.edu.my/id/eprint/9785/ |
| url_provider | http://eprints.utem.edu.my/ |