Development and Characterization of Mesoporous Activated Carbon From Cassia fistula Waste

Waste derived from the Cassia fistula tree, including pods, leaves and bark, was used as a starting material for the synthesis of mesoporous activated carbon (M-AC) through a single-step chemical activation process. Characterization of the samples was confirmed by using SEM, XRD, BET, FTIR and EDX a...

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Main Authors: Hafeez, Bushra, Ullah, Sami, Hayat, Khyzar, Sattar, Rabia, Sanghvi, Gaurav, Khare, Neeraj, Afzaal, Muhammad, Kamilah, Hanisah, Islam, Fakhar, Ndagire, Catherine Tamale
Format: Article
Language:en
Published: John Wiley and Sons Inc 2026
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Online Access:http://psasir.upm.edu.my/id/eprint/124607/1/124607.pdf
http://psasir.upm.edu.my/id/eprint/124607/
https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ansa.70074
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Summary:Waste derived from the Cassia fistula tree, including pods, leaves and bark, was used as a starting material for the synthesis of mesoporous activated carbon (M-AC) through a single-step chemical activation process. Characterization of the samples was confirmed by using SEM, XRD, BET, FTIR and EDX analysis. The porosity of M-AC was confirmed using FTIR and SEM. EDX confirmed that the samples have high carbon content, approximately 60%, and are free from impurities. SEM analysis confirmed that M-AC exhibits heterogeneous morphology with a globular porous surface. XRD analysis confirmed the amorphous nature of M-AC. BET analysis confirmed that the maximum specific surface area of activated carbon was obtained at 1120 m2/g at an impregnation ratio (ZnCl2 solution/C. fistula pods) of 2:1 and a carbonization temperature of 600°C. M-ACP exhibits a total pore volume of 0.90 cm3/g and an average pore size of 4.7 nm.