Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage

Mesoporous ?-alumina with relatively high surface area of 400 m 2/g and pore size of ca. 3.8 nm were successfully prepared using facile and cost-effective method employing sol-gel route at room temperature and atmospheric pressure in the presence of conventional surfactant and fatty alcohol (palm oi...

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Main Authors: Misran H., Aminuddin A.M., Zini F.A.M., Ramesh S.
Other Authors: 6506899840
Format: Conference paper
Published: Electrochemical Society Inc. 2023
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author Misran H.
Aminuddin A.M.
Zini F.A.M.
Ramesh S.
author2 6506899840
author_facet 6506899840
Misran H.
Aminuddin A.M.
Zini F.A.M.
Ramesh S.
author_sort Misran H.
building UNITEN Library
collection Institutional Repository
content_provider Universiti Tenaga Nasional
content_source UNITEN Institutional Repository
continent Asia
country Malaysia
description Mesoporous ?-alumina with relatively high surface area of 400 m 2/g and pore size of ca. 3.8 nm were successfully prepared using facile and cost-effective method employing sol-gel route at room temperature and atmospheric pressure in the presence of conventional surfactant and fatty alcohol (palm oil derived) as template. The limited amount of water gradually added during the synthesis was found to control the rapid hydrolysis rate of the alumina precursors resulting in mesoporous formation. The mesoporosity were retained when changing the surfactant to fatty alcohol. In addition, the materials porosity was made up from framework porosity as well as textural porosity given rise from the aggregations of ?-alumina nanoparticulates. �The Electrochemical Society.
format Conference paper
id my.uniten.dspace-30719
institution Universiti Tenaga Nasional
publishDate 2023
publisher Electrochemical Society Inc.
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spelling my.uniten.dspace-307192023-12-29T15:51:51Z Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage Misran H. Aminuddin A.M. Zini F.A.M. Ramesh S. 6506899840 36981327400 36982594200 41061958200 Alcohols Alumina Atmospheric pressure Cost effectiveness Costs Palm oil Pore size Sol-gel process Sol-gels Surface active agents Alumina precursor Conventional surfactants Cost-effective methods Facile preparation High surface area Hydrolysis rate Nanoparticulates Textural porosity Aluminum oxide Mesoporous ?-alumina with relatively high surface area of 400 m 2/g and pore size of ca. 3.8 nm were successfully prepared using facile and cost-effective method employing sol-gel route at room temperature and atmospheric pressure in the presence of conventional surfactant and fatty alcohol (palm oil derived) as template. The limited amount of water gradually added during the synthesis was found to control the rapid hydrolysis rate of the alumina precursors resulting in mesoporous formation. The mesoporosity were retained when changing the surfactant to fatty alcohol. In addition, the materials porosity was made up from framework porosity as well as textural porosity given rise from the aggregations of ?-alumina nanoparticulates. �The Electrochemical Society. Final 2023-12-29T07:51:51Z 2023-12-29T07:51:51Z 2010 Conference paper 10.1149/1.3491774 2-s2.0-79959441228 https://www.scopus.com/inward/record.uri?eid=2-s2.0-79959441228&doi=10.1149%2f1.3491774&partnerID=40&md5=126cb057a47fae3e998799bb82e9eae4 https://irepository.uniten.edu.my/handle/123456789/30719 28 7 57 65 Electrochemical Society Inc. Scopus
spellingShingle Alcohols
Alumina
Atmospheric pressure
Cost effectiveness
Costs
Palm oil
Pore size
Sol-gel process
Sol-gels
Surface active agents
Alumina precursor
Conventional surfactants
Cost-effective methods
Facile preparation
High surface area
Hydrolysis rate
Nanoparticulates
Textural porosity
Aluminum oxide
Misran H.
Aminuddin A.M.
Zini F.A.M.
Ramesh S.
Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
title Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
title_full Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
title_fullStr Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
title_full_unstemmed Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
title_short Facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
title_sort facile preparation and characterizations of potential low-cost nanostructured materials for energy gas storage
topic Alcohols
Alumina
Atmospheric pressure
Cost effectiveness
Costs
Palm oil
Pore size
Sol-gel process
Sol-gels
Surface active agents
Alumina precursor
Conventional surfactants
Cost-effective methods
Facile preparation
High surface area
Hydrolysis rate
Nanoparticulates
Textural porosity
Aluminum oxide
url_provider http://dspace.uniten.edu.my/