Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review

This paper reviews the application of various modes of solid-phase microextraction (SPME) for the analysis of pesticide residues in fruits and vegetables. SPME is a simple extraction technique that eliminates the use of solvent, and it is applied for the analysis of both volatile and nonvolatile pes...

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Main Authors: Abdulra'uf L.B., Chai M.K., Tan G.H.
Other Authors: 55180709700
Format: Review
Published: AOAC International 2023
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author Abdulra'uf L.B.
Chai M.K.
Tan G.H.
author2 55180709700
author_facet 55180709700
Abdulra'uf L.B.
Chai M.K.
Tan G.H.
author_sort Abdulra'uf L.B.
building UNITEN Library
collection Institutional Repository
content_provider Universiti Tenaga Nasional
content_source UNITEN Institutional Repository
continent Asia
country Malaysia
description This paper reviews the application of various modes of solid-phase microextraction (SPME) for the analysis of pesticide residues in fruits and vegetables. SPME is a simple extraction technique that eliminates the use of solvent, and it is applied for the analysis of both volatile and nonvolatile pesticides. SPME has been successfully coupled to both GC and LC. The coupling with GC has been straightforward and requires little modification of existing equipment, but interfacing with LC has proved challenging. The external standard calibration technique is widely used for quantification, while standard addition and internal or surrogate standards are mainly used to account for matrix effects. All parameters that affect the extraction of pesticide residues from fruits and vegetables, and therefore need to be optimized, are also reviewed. Details of the characteristics of analytical procedures and new trends in fiber production using sol-gel technology and molecularly imprinted polymers are discussed.
format Review
id my.uniten.dspace-29478
institution Universiti Tenaga Nasional
publishDate 2023
publisher AOAC International
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spelling my.uniten.dspace-294782023-12-28T14:30:11Z Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review Abdulra'uf L.B. Chai M.K. Tan G.H. 55180709700 24172523100 7202393048 Fruits Pesticides Sol-gels Vegetables Analytical procedure External standards Extraction techniques Fruits and vegetables Molecularly Imprinted Polymer Sol-gel technology Solid-phase microextraction Standard addition Extraction This paper reviews the application of various modes of solid-phase microextraction (SPME) for the analysis of pesticide residues in fruits and vegetables. SPME is a simple extraction technique that eliminates the use of solvent, and it is applied for the analysis of both volatile and nonvolatile pesticides. SPME has been successfully coupled to both GC and LC. The coupling with GC has been straightforward and requires little modification of existing equipment, but interfacing with LC has proved challenging. The external standard calibration technique is widely used for quantification, while standard addition and internal or surrogate standards are mainly used to account for matrix effects. All parameters that affect the extraction of pesticide residues from fruits and vegetables, and therefore need to be optimized, are also reviewed. Details of the characteristics of analytical procedures and new trends in fiber production using sol-gel technology and molecularly imprinted polymers are discussed. Final 2023-12-28T06:30:11Z 2023-12-28T06:30:11Z 2012 Review 10.5740/jaoacint.SGE_Abdulrauf 2-s2.0-84867857873 https://www.scopus.com/inward/record.uri?eid=2-s2.0-84867857873&doi=10.5740%2fjaoacint.SGE_Abdulrauf&partnerID=40&md5=6fb3f271fdd4ea3090d35857ca99ae8c https://irepository.uniten.edu.my/handle/123456789/29478 95 5 1272 1290 All Open Access; Bronze Open Access AOAC International Scopus
spellingShingle Fruits
Pesticides
Sol-gels
Vegetables
Analytical procedure
External standards
Extraction techniques
Fruits and vegetables
Molecularly Imprinted Polymer
Sol-gel technology
Solid-phase microextraction
Standard addition
Extraction
Abdulra'uf L.B.
Chai M.K.
Tan G.H.
Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review
title Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review
title_full Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review
title_fullStr Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review
title_full_unstemmed Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review
title_short Applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: A review
title_sort applications of solid-phase microextraction for the analysis of pesticide residues in fruits and vegetables: a review
topic Fruits
Pesticides
Sol-gels
Vegetables
Analytical procedure
External standards
Extraction techniques
Fruits and vegetables
Molecularly Imprinted Polymer
Sol-gel technology
Solid-phase microextraction
Standard addition
Extraction
url_provider http://dspace.uniten.edu.my/