Influence of Microstructural Effect on Microvickers Hardness Properties of SiO2-Na2O-CaO (SNC) Waste Based Glass-ceramic

There are a lot of waste materials consist of silicate based such as coal combustion ash, slag from steel production, fly ash, mud, as well as glass cullet or mixtures to produce glass-ceramics. This research work using clam shell (CS) ash and soda-lime-silica (SLS) waste glass powder for fabrica...

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Bibliographic Details
Main Authors: Nur Fadilah, Baharuddin Pallan, N F, Adnin, K A, Matori, Mansor, Hashim, F M, Idris, Idza Riati, Ibrahim, S N A, Rusly, M Z A, Khiri, Rodziah, Nazlan, N Hapishah, Abdullah, M S E, Shafie, R S, Aziz, Z N, Alassan, N, Zainuddin, N Faizah, Baharuddin Pallan, Noraziah, Ahmad, Maria, Nuid
Format: Article
Language:en
Published: IOP Publishing Ltd 2018
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Online Access:http://ir.unimas.my/id/eprint/35455/1/Baharuddin_Pallan_2018_J._Phys.__Conf._Ser._1083_012008.pdf
http://ir.unimas.my/id/eprint/35455/
https://iopscience.iop.org/article/10.1088/1742-6596/1083/1/012008
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Summary:There are a lot of waste materials consist of silicate based such as coal combustion ash, slag from steel production, fly ash, mud, as well as glass cullet or mixtures to produce glass-ceramics. This research work using clam shell (CS) ash and soda-lime-silica (SLS) waste glass powder for fabricating novel SiO2-Na2O-CaO (SNC) glass-ceramic. The samples were composed of SLS (50%), Na2CO3 (30%), and CS (20%) in weight percentage via conventional melt-quenching technique and solid-state sintering technique. The samples were investigated via X-Ray Diffractometer (XRD), Field emission microscope (FESEM), and microvickers hardness tester. The samples were sintered at 550-950 °C to investigate the influence of microstructural effect on microvickers hardness properties at applied force 0.5 and 1.0 kgf. The optimal Vickers hardness properties at sintering temperature 850 °C due to high crystallization of SiO2 phase from the residual glass and CaO content enhanced the viscosity flow, high compactness of particles arrangement and densification of sample.