Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process

The objective of this research is to study the behaviour of Non-newtonian flow for hollow fiber membrane spinning process. Inorganic membrane was chosen as the hollow fiber membrane material to be developed as it has certain advantage compared to organic hollow fiber membrane. Kaolin was selected a...

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Main Author: Mohd Suffian Misaran
Format: Research Report
Language:en
Published: Universiti Malaysia Sabah 2013
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Online Access:https://eprints.ums.edu.my/id/eprint/22849/1/Behaviours%20of%20non%20newtonian%20flow%20mechanism%20through%20hollow%20tube%20spinneret%20for%20hollow%20fiber%20membrane%20spinning%20process.pdf
https://eprints.ums.edu.my/id/eprint/22849/
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author Mohd Suffian Misaran
author_facet Mohd Suffian Misaran
author_sort Mohd Suffian Misaran
building UMS Library
collection Institutional Repository
content_provider Universiti Malaysia Sabah
content_source UMS Institutional Repository
continent Asia
country Malaysia
description The objective of this research is to study the behaviour of Non-newtonian flow for hollow fiber membrane spinning process. Inorganic membrane was chosen as the hollow fiber membrane material to be developed as it has certain advantage compared to organic hollow fiber membrane. Kaolin was selected as the primary material while Polyether Sulfone (PESt) was used as the binder agent, NMP was used as solvent in its original form. To decouple the effect of other spinning factors and isolate only to viscosity and spinneret dimension, the spinning was done using dry/wet spinning process without take-up mechanism. Then, the hollow fiber membrane underwent sintering process to remove the PESf binder from the ceramic structure. Scanning electron microscopy (SEM) method was used to characterize the hollow fiber membrane structure. While spinning the hollow fiber membrane, kaolin suspension was extruded in a complicated channel within a tube-orifice spinneret. The suspension will subject to shear stress which may Influence the fiber's formation, morphology and separation performance due to chain entanglement. Thus, CFD study was conducted to simulate flow behavior in the spinneret and correlated with morphology of hollow fiber membrane. In this study, we found that the addition of kaolin onto PESf solution enhance the non-newtonian behavior and crossly resemblance the pseudo-plastic flow. Simulation data also shows that there is a high correlation between fluid stability and hollow fiber morphology. A much stable flow was observed at longer retention time in the spinneret annulus and the hollow fiber yields better structural integrity. Improvement made on spinneret design yields better concentricity structure on the hollow fiber as well.
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institution Universiti Malaysia Sabah
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publisher Universiti Malaysia Sabah
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spelling my.ums.eprints-228492019-07-19T06:57:34Z https://eprints.ums.edu.my/id/eprint/22849/ Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process Mohd Suffian Misaran TJ Mechanical engineering and machinery The objective of this research is to study the behaviour of Non-newtonian flow for hollow fiber membrane spinning process. Inorganic membrane was chosen as the hollow fiber membrane material to be developed as it has certain advantage compared to organic hollow fiber membrane. Kaolin was selected as the primary material while Polyether Sulfone (PESt) was used as the binder agent, NMP was used as solvent in its original form. To decouple the effect of other spinning factors and isolate only to viscosity and spinneret dimension, the spinning was done using dry/wet spinning process without take-up mechanism. Then, the hollow fiber membrane underwent sintering process to remove the PESf binder from the ceramic structure. Scanning electron microscopy (SEM) method was used to characterize the hollow fiber membrane structure. While spinning the hollow fiber membrane, kaolin suspension was extruded in a complicated channel within a tube-orifice spinneret. The suspension will subject to shear stress which may Influence the fiber's formation, morphology and separation performance due to chain entanglement. Thus, CFD study was conducted to simulate flow behavior in the spinneret and correlated with morphology of hollow fiber membrane. In this study, we found that the addition of kaolin onto PESf solution enhance the non-newtonian behavior and crossly resemblance the pseudo-plastic flow. Simulation data also shows that there is a high correlation between fluid stability and hollow fiber morphology. A much stable flow was observed at longer retention time in the spinneret annulus and the hollow fiber yields better structural integrity. Improvement made on spinneret design yields better concentricity structure on the hollow fiber as well. Universiti Malaysia Sabah 2013 Research Report NonPeerReviewed text en https://eprints.ums.edu.my/id/eprint/22849/1/Behaviours%20of%20non%20newtonian%20flow%20mechanism%20through%20hollow%20tube%20spinneret%20for%20hollow%20fiber%20membrane%20spinning%20process.pdf Mohd Suffian Misaran (2013) Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process. (Unpublished)
spellingShingle TJ Mechanical engineering and machinery
Mohd Suffian Misaran
Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
title Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
title_full Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
title_fullStr Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
title_full_unstemmed Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
title_short Behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
title_sort behaviours of non-newtonian flow mechanism through hollow tube spinneret for hollow fiber membrane spinning process
topic TJ Mechanical engineering and machinery
url https://eprints.ums.edu.my/id/eprint/22849/1/Behaviours%20of%20non%20newtonian%20flow%20mechanism%20through%20hollow%20tube%20spinneret%20for%20hollow%20fiber%20membrane%20spinning%20process.pdf
https://eprints.ums.edu.my/id/eprint/22849/
url_provider http://eprints.ums.edu.my/