Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol
Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit. The effects of temperature and solvent concentration on yield, particle size distributi...
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| Format: | Article |
| Language: | en en |
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Elsevier
2012
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| Online Access: | http://umpir.ump.edu.my/id/eprint/6790/1/Effects_of_temperature_and_solvent_concentration_on_the_solvent_crystallization_of.pdf http://umpir.ump.edu.my/id/eprint/6790/4/Particuology%2010.pdf http://umpir.ump.edu.my/id/eprint/6790/ http://www.sciencedirect.com/science/article/pii/S1674200111001714# |
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| author | Koay, Gregory F. L. Chuaha, Teong-Guan Sumaiya, Zainal Abidin Salmiah, Ahmad Choonga, Thomas S. Y. |
| author_facet | Koay, Gregory F. L. Chuaha, Teong-Guan Sumaiya, Zainal Abidin Salmiah, Ahmad Choonga, Thomas S. Y. |
| author_sort | Koay, Gregory F. L. |
| building | UMPSA Library |
| collection | Institutional Repository |
| content_provider | Universiti Malaysia Pahang Al-Sultan Abdullah |
| content_source | UMPSA Institutional Repository |
| continent | Asia |
| country | Malaysia |
| description | Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit. The effects of temperature and solvent concentration on yield, particle size distribution and purity were studied. The purity was higher, while the yield and particle size were lower and smaller, respectively, at higher temperature and solvent concentration. The solvent crystallization process efficiency was rated at 66–69% when carried out with 70–80% isopropyl alcohol at 20 ◦C. |
| format | Article |
| id | my.ump.umpir.6790 |
| institution | Universiti Malaysia Pahang |
| language | en en |
| publishDate | 2012 |
| publisher | Elsevier |
| record_format | eprints |
| spelling | my.ump.umpir.67902018-04-18T01:14:08Z http://umpir.ump.edu.my/id/eprint/6790/ Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol Koay, Gregory F. L. Chuaha, Teong-Guan Sumaiya, Zainal Abidin Salmiah, Ahmad Choonga, Thomas S. Y. QD Chemistry Palm-based dihydroxystearic acid of 69.55% purity was produced in a 500-kg-per-batch operation pilot plant and purified through solvent crystallization in a custom fabricated simultaneous batch crystallizer unit. The effects of temperature and solvent concentration on yield, particle size distribution and purity were studied. The purity was higher, while the yield and particle size were lower and smaller, respectively, at higher temperature and solvent concentration. The solvent crystallization process efficiency was rated at 66–69% when carried out with 70–80% isopropyl alcohol at 20 ◦C. Elsevier 2012 Article PeerReviewed application/pdf en http://umpir.ump.edu.my/id/eprint/6790/1/Effects_of_temperature_and_solvent_concentration_on_the_solvent_crystallization_of.pdf application/pdf en http://umpir.ump.edu.my/id/eprint/6790/4/Particuology%2010.pdf Koay, Gregory F. L. and Chuaha, Teong-Guan and Sumaiya, Zainal Abidin and Salmiah, Ahmad and Choonga, Thomas S. Y. (2012) Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol. Particuology, 10 (1). pp. 127-131. (Published) http://www.sciencedirect.com/science/article/pii/S1674200111001714# 10.1016/j.partic.2011.04.011 |
| spellingShingle | QD Chemistry Koay, Gregory F. L. Chuaha, Teong-Guan Sumaiya, Zainal Abidin Salmiah, Ahmad Choonga, Thomas S. Y. Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| title | Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| title_full | Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| title_fullStr | Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| title_full_unstemmed | Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| title_short | Effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| title_sort | effects of temperature and solvent concentration on the solvent crystallization of palm-based dihydroxystearic acid with isopropyl alcohol |
| topic | QD Chemistry |
| url | http://umpir.ump.edu.my/id/eprint/6790/1/Effects_of_temperature_and_solvent_concentration_on_the_solvent_crystallization_of.pdf http://umpir.ump.edu.my/id/eprint/6790/4/Particuology%2010.pdf http://umpir.ump.edu.my/id/eprint/6790/ http://www.sciencedirect.com/science/article/pii/S1674200111001714# |
| url_provider | http://umpir.ump.edu.my/ |