Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites

This paper focuses on the effect of sintering temperature on the structural, microstructural and magnetic properties of cobalt ferrite (CF). CF with sintering temperatures of 600 ℃ to 1400 ℃, was synthesized using the oxide mixture route technique. The structural and microstructural development of t...

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Main Authors: Nurul Atiqah Mohd, Pauzi, Rodziah, Nazlan, Nurul Masliana, Khairil Anuar, Mohamad Ashry, Jusoh, Idza Riati, Ibrahim, Farah Nabilah, Shafiee
Format: Conference or Workshop Item
Language:en
en
Published: Elsevier Ltd 2021
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Online Access:http://umpir.ump.edu.my/id/eprint/35580/1/Sintering%20temperature%20dependence%20on%20evolving%20microstructure%20and%20magnetic.pdf
http://umpir.ump.edu.my/id/eprint/35580/2/Sintering%20temperature%20dependence%20on%20evolving%20microstructure%20and%20magnetic%20characteristics%20of%20cobalt%20ferrites_Abs.pdf
http://umpir.ump.edu.my/id/eprint/35580/
https://doi.org/10.1016/j.matpr.2021.11.640
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_version_ 1831528930462400512
author Nurul Atiqah Mohd, Pauzi
Rodziah, Nazlan
Nurul Masliana, Khairil Anuar
Mohamad Ashry, Jusoh
Idza Riati, Ibrahim
Farah Nabilah, Shafiee
author_facet Nurul Atiqah Mohd, Pauzi
Rodziah, Nazlan
Nurul Masliana, Khairil Anuar
Mohamad Ashry, Jusoh
Idza Riati, Ibrahim
Farah Nabilah, Shafiee
author_sort Nurul Atiqah Mohd, Pauzi
building UMPSA Library
collection Institutional Repository
content_provider Universiti Malaysia Pahang Al-Sultan Abdullah
content_source UMPSA Institutional Repository
continent Asia
country Malaysia
description This paper focuses on the effect of sintering temperature on the structural, microstructural and magnetic properties of cobalt ferrite (CF). CF with sintering temperatures of 600 ℃ to 1400 ℃, was synthesized using the oxide mixture route technique. The structural and microstructural development of the samples were investigated using X-Ray Diffractometer, Transmission Electron Microscope and Scanning Electron Microscope, while the magnetic dynamic properties of the samples were analyzed using Impedance/ Material Analyzer over 1 MHz to 1 GHz. The results show that the complex permeability which include the real permeability and loss factor of the samples at 10 MHz have shown an increase in their values through increasing the sintering temperature. As sintering temperature acted as a temporary agent for structural and microstructural development, the improvement of crystallization and microstructure by heat treatment, contributed to a single CF phase formation and grain growth, resulting in the removal of porosity and microstrain in the samples. This in turn enhanced the superexchange interactions between magnetic moments via elimination of domain wall pinning point, thus contributes to the improvement of magnetic characteristics of the samples.
format Conference or Workshop Item
id my.ump.umpir.35580
institution Universiti Malaysia Pahang
language en
en
publishDate 2021
publisher Elsevier Ltd
record_format eprints
spelling my.ump.umpir.355802023-02-21T03:16:43Z http://umpir.ump.edu.my/id/eprint/35580/ Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites Nurul Atiqah Mohd, Pauzi Rodziah, Nazlan Nurul Masliana, Khairil Anuar Mohamad Ashry, Jusoh Idza Riati, Ibrahim Farah Nabilah, Shafiee Q Science (General) T Technology (General) TP Chemical technology This paper focuses on the effect of sintering temperature on the structural, microstructural and magnetic properties of cobalt ferrite (CF). CF with sintering temperatures of 600 ℃ to 1400 ℃, was synthesized using the oxide mixture route technique. The structural and microstructural development of the samples were investigated using X-Ray Diffractometer, Transmission Electron Microscope and Scanning Electron Microscope, while the magnetic dynamic properties of the samples were analyzed using Impedance/ Material Analyzer over 1 MHz to 1 GHz. The results show that the complex permeability which include the real permeability and loss factor of the samples at 10 MHz have shown an increase in their values through increasing the sintering temperature. As sintering temperature acted as a temporary agent for structural and microstructural development, the improvement of crystallization and microstructure by heat treatment, contributed to a single CF phase formation and grain growth, resulting in the removal of porosity and microstrain in the samples. This in turn enhanced the superexchange interactions between magnetic moments via elimination of domain wall pinning point, thus contributes to the improvement of magnetic characteristics of the samples. Elsevier Ltd 2021 Conference or Workshop Item PeerReviewed pdf en http://umpir.ump.edu.my/id/eprint/35580/1/Sintering%20temperature%20dependence%20on%20evolving%20microstructure%20and%20magnetic.pdf pdf en http://umpir.ump.edu.my/id/eprint/35580/2/Sintering%20temperature%20dependence%20on%20evolving%20microstructure%20and%20magnetic%20characteristics%20of%20cobalt%20ferrites_Abs.pdf Nurul Atiqah Mohd, Pauzi and Rodziah, Nazlan and Nurul Masliana, Khairil Anuar and Mohamad Ashry, Jusoh and Idza Riati, Ibrahim and Farah Nabilah, Shafiee (2021) Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites. In: Materials Today: Proceedings; 3rd Symposium on Industrial Science and Technology, SISTEC 2021 , 25 - 26 August 2021 , Kuantan, Pahang. pp. 1420-1425., 51 (2). ISSN 2214-7853 (Published) https://doi.org/10.1016/j.matpr.2021.11.640
spellingShingle Q Science (General)
T Technology (General)
TP Chemical technology
Nurul Atiqah Mohd, Pauzi
Rodziah, Nazlan
Nurul Masliana, Khairil Anuar
Mohamad Ashry, Jusoh
Idza Riati, Ibrahim
Farah Nabilah, Shafiee
Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
title Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
title_full Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
title_fullStr Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
title_full_unstemmed Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
title_short Sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
title_sort sintering temperature dependence on evolving microstructure and magnetic characteristics of cobalt ferrites
topic Q Science (General)
T Technology (General)
TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/35580/1/Sintering%20temperature%20dependence%20on%20evolving%20microstructure%20and%20magnetic.pdf
http://umpir.ump.edu.my/id/eprint/35580/2/Sintering%20temperature%20dependence%20on%20evolving%20microstructure%20and%20magnetic%20characteristics%20of%20cobalt%20ferrites_Abs.pdf
http://umpir.ump.edu.my/id/eprint/35580/
https://doi.org/10.1016/j.matpr.2021.11.640
url_provider http://umpir.ump.edu.my/