Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method

This paper studies on the effect of synthesis parameters towards the performance of superabsorbent carbonaceous polymer (SPC) via inverse suspension polymerization method. The SPC consists of acrylic acid, acrylamide, and carbon filler. In this work, four independent factors (synthesis parameters) i...

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Main Authors: S. N. Ainda, Mazlan, Saidatul Shima, Jamari
Format: Conference or Workshop Item
Language:en
Published: IOP Publishing 2019
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Online Access:http://umpir.ump.edu.my/id/eprint/25399/1/Factorial%20experimental%20design%20for%20superabsorbent%20carbonaceous.pdf
http://umpir.ump.edu.my/id/eprint/25399/
https://doi.org/10.1088/1757-899X/523/1/012021
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author S. N. Ainda, Mazlan
Saidatul Shima, Jamari
author_facet S. N. Ainda, Mazlan
Saidatul Shima, Jamari
author_sort S. N. Ainda, Mazlan
building UMPSA Library
collection Institutional Repository
content_provider Universiti Malaysia Pahang Al-Sultan Abdullah
content_source UMPSA Institutional Repository
continent Asia
country Malaysia
description This paper studies on the effect of synthesis parameters towards the performance of superabsorbent carbonaceous polymer (SPC) via inverse suspension polymerization method. The SPC consists of acrylic acid, acrylamide, and carbon filler. In this work, four independent factors (synthesis parameters) i.e. the content of carbon filler, the content of initiator, the content of crosslinker and reaction temperature that affecting the water absorbency of SPC was investigated. A 24 full factorial design was used to investigate the effect of independent factors as well as the interaction factors on the water absorbency of SPC. Apart from reaction temperature, other factors were shown to have the significant effect on the water absorbency of SPC. The results showed the order of significance: initiator's content > crosslinker's content > carbon filler's content > reaction temperature. Meanwhile, interaction factor of carbon filler's and crosslinker's content had the strongest effect on the water absorbency amongst the other interactions. The highest water absorbency of the SPC was achieved at the conditions (filler's content (A): 0.05wt%; initiator's content (B): 0.10wt%; crosslinker's content (C): 0.001wt%, and reaction temperature: 70°C).
format Conference or Workshop Item
id my.ump.umpir.25399
institution Universiti Malaysia Pahang
language en
publishDate 2019
publisher IOP Publishing
record_format eprints
spelling my.ump.umpir.253992020-12-01T07:06:40Z http://umpir.ump.edu.my/id/eprint/25399/ Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method S. N. Ainda, Mazlan Saidatul Shima, Jamari TP Chemical technology This paper studies on the effect of synthesis parameters towards the performance of superabsorbent carbonaceous polymer (SPC) via inverse suspension polymerization method. The SPC consists of acrylic acid, acrylamide, and carbon filler. In this work, four independent factors (synthesis parameters) i.e. the content of carbon filler, the content of initiator, the content of crosslinker and reaction temperature that affecting the water absorbency of SPC was investigated. A 24 full factorial design was used to investigate the effect of independent factors as well as the interaction factors on the water absorbency of SPC. Apart from reaction temperature, other factors were shown to have the significant effect on the water absorbency of SPC. The results showed the order of significance: initiator's content > crosslinker's content > carbon filler's content > reaction temperature. Meanwhile, interaction factor of carbon filler's and crosslinker's content had the strongest effect on the water absorbency amongst the other interactions. The highest water absorbency of the SPC was achieved at the conditions (filler's content (A): 0.05wt%; initiator's content (B): 0.10wt%; crosslinker's content (C): 0.001wt%, and reaction temperature: 70°C). IOP Publishing 2019 Conference or Workshop Item PeerReviewed pdf en cc_by http://umpir.ump.edu.my/id/eprint/25399/1/Factorial%20experimental%20design%20for%20superabsorbent%20carbonaceous.pdf S. N. Ainda, Mazlan and Saidatul Shima, Jamari (2019) Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method. In: IOP Conference Series: Materials Science and Engineering, The 8th Annual International Conference (AIC) 2018 on Science and Engineering , 12-14 September 2018 , Aceh, Indonesia. pp. 1-6., 523 (012021). ISSN 1757-899X (Published) https://doi.org/10.1088/1757-899X/523/1/012021
spellingShingle TP Chemical technology
S. N. Ainda, Mazlan
Saidatul Shima, Jamari
Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
title Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
title_full Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
title_fullStr Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
title_full_unstemmed Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
title_short Factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
title_sort factorial experimental design for superabsorbent carbonaceous polymer through inverse suspension polymerization method
topic TP Chemical technology
url http://umpir.ump.edu.my/id/eprint/25399/1/Factorial%20experimental%20design%20for%20superabsorbent%20carbonaceous.pdf
http://umpir.ump.edu.my/id/eprint/25399/
https://doi.org/10.1088/1757-899X/523/1/012021
url_provider http://umpir.ump.edu.my/