N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate

The title compound, C(16)H(16)N(2)O(6)center dot C(2)H(5)OH, was synthesized from 3,4,5-trihydroxybenzoylhydrazide and 2,4-dimethoxybenzaldehyde in ethanol. The compound is not planar, with the two aromatic planes of the two aromatic rings twisted by 15.6 ( 1)degrees. The hydroxy groups are involved...

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Main Authors: Alhadi, A.A., Abdulla, M.A., Robinson, W.T., Ali, Hapipah Mohd, Saharin, S.M.
Format: Article
Published: International Union of Crystallography 2009
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Online Access:http://eprints.um.edu.my/5421/
http://scripts.iucr.org/cgi-bin/paper?S1600536809018947
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author Alhadi, A.A.
Abdulla, M.A.
Robinson, W.T.
Ali, Hapipah Mohd
Saharin, S.M.
author_facet Alhadi, A.A.
Abdulla, M.A.
Robinson, W.T.
Ali, Hapipah Mohd
Saharin, S.M.
author_sort Alhadi, A.A.
building UM Library
collection Institutional Repository
content_provider Universiti Malaya
content_source UM Research Repository
continent Asia
country Malaysia
description The title compound, C(16)H(16)N(2)O(6)center dot C(2)H(5)OH, was synthesized from 3,4,5-trihydroxybenzoylhydrazide and 2,4-dimethoxybenzaldehyde in ethanol. The compound is not planar, with the two aromatic planes of the two aromatic rings twisted by 15.6 ( 1)degrees. The hydroxy groups are involved in both intramolecular O-H center dot center dot center dot O and intermolecular O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonds and a C-H center dot center dot center dot O interaction also occurs.
format Article
id my.um.eprints-5421
institution Universiti Malaya
publishDate 2009
publisher International Union of Crystallography
record_format eprints
spelling my.um.eprints-54212019-01-29T08:43:43Z http://eprints.um.edu.my/5421/ N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate Alhadi, A.A. Abdulla, M.A. Robinson, W.T. Ali, Hapipah Mohd Saharin, S.M. QD Chemistry The title compound, C(16)H(16)N(2)O(6)center dot C(2)H(5)OH, was synthesized from 3,4,5-trihydroxybenzoylhydrazide and 2,4-dimethoxybenzaldehyde in ethanol. The compound is not planar, with the two aromatic planes of the two aromatic rings twisted by 15.6 ( 1)degrees. The hydroxy groups are involved in both intramolecular O-H center dot center dot center dot O and intermolecular O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonds and a C-H center dot center dot center dot O interaction also occurs. International Union of Crystallography 2009 Article PeerReviewed Alhadi, A.A. and Abdulla, M.A. and Robinson, W.T. and Ali, Hapipah Mohd and Saharin, S.M. (2009) N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate. Acta Crystallographica Section E: Structure Reports Online, 65. O1373-U2699. ISSN 1600-5368, DOI https://doi.org/10.1107/s1600536809018947 <https://doi.org/10.1107/s1600536809018947>. http://scripts.iucr.org/cgi-bin/paper?S1600536809018947 10.1107/s1600536809018947
spellingShingle QD Chemistry
Alhadi, A.A.
Abdulla, M.A.
Robinson, W.T.
Ali, Hapipah Mohd
Saharin, S.M.
N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
title N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
title_full N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
title_fullStr N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
title_full_unstemmed N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
title_short N '-(2,4-Dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
title_sort n '-(2,4-dimethoxybenzylidene)-3,4,5-trihydroxybenzohydrazide ethanol solvate
topic QD Chemistry
url http://eprints.um.edu.my/5421/
http://scripts.iucr.org/cgi-bin/paper?S1600536809018947
url_provider http://eprints.um.edu.my/