Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide)
A new hydrazide Shiff base ligand GHL1 (5-bromo-2-hydroxybezylidene)-3,4,5-trihydroxybenzohydrazide) was prepared by refluxing of trihydroxybenzhydrazide with an ethanolic of 5-bromo-2-hydroxybenzaldehyde. The ligand reacted with Ni(II), Cu(II), Zn(II) and Cd(II) (acetate salts). All the complexes w...
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2012
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| author | Alhadi, A.A. Abdullah, M.A. Ali, Hapipah Mohd Yehye, W.A. Shaker, S.A. |
| author_facet | Alhadi, A.A. Abdullah, M.A. Ali, Hapipah Mohd Yehye, W.A. Shaker, S.A. |
| author_sort | Alhadi, A.A. |
| building | UM Library |
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| content_provider | Universiti Malaya |
| content_source | UM Research Repository |
| continent | Asia |
| country | Malaysia |
| description | A new hydrazide Shiff base ligand GHL1 (5-bromo-2-hydroxybezylidene)-3,4,5-trihydroxybenzohydrazide) was prepared by refluxing of trihydroxybenzhydrazide with an ethanolic of 5-bromo-2-hydroxybenzaldehyde. The ligand reacted with Ni(II), Cu(II), Zn(II) and Cd(II) (acetate salts). All the complexes were characterized by elemental analysis, molar conductivity, TGA, UV-Vis and FT-IR spectral studies. All the complexes have octahedral geometry except Ni(II) complex which has tetrahedral geometry. |
| format | Article |
| id | my.um.eprints-5152 |
| institution | Universiti Malaya |
| publishDate | 2012 |
| record_format | eprints |
| spelling | my.um.eprints-51522019-01-30T01:08:59Z http://eprints.um.edu.my/5152/ Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) Alhadi, A.A. Abdullah, M.A. Ali, Hapipah Mohd Yehye, W.A. Shaker, S.A. QD Chemistry A new hydrazide Shiff base ligand GHL1 (5-bromo-2-hydroxybezylidene)-3,4,5-trihydroxybenzohydrazide) was prepared by refluxing of trihydroxybenzhydrazide with an ethanolic of 5-bromo-2-hydroxybenzaldehyde. The ligand reacted with Ni(II), Cu(II), Zn(II) and Cd(II) (acetate salts). All the complexes were characterized by elemental analysis, molar conductivity, TGA, UV-Vis and FT-IR spectral studies. All the complexes have octahedral geometry except Ni(II) complex which has tetrahedral geometry. 2012 Article PeerReviewed Alhadi, A.A. and Abdullah, M.A. and Ali, Hapipah Mohd and Yehye, W.A. and Shaker, S.A. (2012) Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide). Bulletin of the Chemical Society of Ethiopia, 26 (1). pp. 95-101. ISSN 1011-3924, DOI https://doi.org/10.4314/bcse.v26i1.10 <https://doi.org/10.4314/bcse.v26i1.10>. http://www.ajol.info/index.php/bcse/article/viewFile/72964/61855 10.4314/bcse.v26i1.10 |
| spellingShingle | QD Chemistry Alhadi, A.A. Abdullah, M.A. Ali, Hapipah Mohd Yehye, W.A. Shaker, S.A. Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) |
| title | Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) |
| title_full | Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) |
| title_fullStr | Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) |
| title_full_unstemmed | Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) |
| title_short | Synthesis, magnetic and spectroscopic studies of Ni(Ii), Cu(Ii), Zn(Ii) and Cd(Ii) complexes of a newly Schiff Base derived from 5-Bromo-2-Hydroxybezylidene)-3,4,5-Trihydroxybenzohydrazide) |
| title_sort | synthesis, magnetic and spectroscopic studies of ni(ii), cu(ii), zn(ii) and cd(ii) complexes of a newly schiff base derived from 5-bromo-2-hydroxybezylidene)-3,4,5-trihydroxybenzohydrazide) |
| topic | QD Chemistry |
| url | http://eprints.um.edu.my/5152/ http://www.ajol.info/index.php/bcse/article/viewFile/72964/61855 |
| url_provider | http://eprints.um.edu.my/ |