Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /

Titania nanotubes (TiNT) has gained much interest as it has high surface area and fewer grain boundaries. In order to enhance the photoelectrochemical properties of TiNT, modification has been carried out to dope silver on TiNT. In this study, a combination of electrochemical anodisation and a photo...

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Main Authors: Lim, Ying Pei, Kanakaraju, Devagi, Lim, Ying Chin
Format: Article
Language:en
Published: Universiti Teknologi MARA Shah Alam 2020
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Online Access:https://ir.uitm.edu.my/id/eprint/43485/1/43485.pdf
https://ir.uitm.edu.my/id/eprint/43485/
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author Lim, Ying Pei
Kanakaraju, Devagi
Lim, Ying Chin
author_facet Lim, Ying Pei
Kanakaraju, Devagi
Lim, Ying Chin
author_sort Lim, Ying Pei
building Tun Abdul Razak Library
collection Institutional Repository
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
continent Asia
country Malaysia
description Titania nanotubes (TiNT) has gained much interest as it has high surface area and fewer grain boundaries. In order to enhance the photoelectrochemical properties of TiNT, modification has been carried out to dope silver on TiNT. In this study, a combination of electrochemical anodisation and a photochemical reduction was employed to fabricate silver supported on titania nanotubes (AgTiNT). TiNT was synthesized via anodisation of titanium plate in a two-electrode system containing ethylene glycol and ammonium fluoride. Then, the silver particles were deposited on TiNT by immersion in various concentrations of silver precursor solution followed by ultraviolet light radiation. The prepared samples were characterized using field emission scanning electron microscopy (FESEM) for morphology, x-ray diffractometry (XRD) for crystal structure and energy dispersive x-ray (EDX) to determine the element content. TiNT demonstrated a well-ordered structure, but the nanotubes tend to clump together upon deposition of Ag. The effect of Ag deposition on the photoelectrochemical performance of TiNT was studied where almost one-fold enhancement in the photoelectrochemical property was observed for AgTiNT compared to pure TiNT.
format Article
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institution Universiti Teknologi Mara
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publisher Universiti Teknologi MARA Shah Alam
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spelling my.uitm.ir-434852021-03-12T09:08:08Z https://ir.uitm.edu.my/id/eprint/43485/ Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration / mjcet Lim, Ying Pei Kanakaraju, Devagi Lim, Ying Chin Carbon nanotubes. Nanoparticles. Nanostructured materials Titania nanotubes (TiNT) has gained much interest as it has high surface area and fewer grain boundaries. In order to enhance the photoelectrochemical properties of TiNT, modification has been carried out to dope silver on TiNT. In this study, a combination of electrochemical anodisation and a photochemical reduction was employed to fabricate silver supported on titania nanotubes (AgTiNT). TiNT was synthesized via anodisation of titanium plate in a two-electrode system containing ethylene glycol and ammonium fluoride. Then, the silver particles were deposited on TiNT by immersion in various concentrations of silver precursor solution followed by ultraviolet light radiation. The prepared samples were characterized using field emission scanning electron microscopy (FESEM) for morphology, x-ray diffractometry (XRD) for crystal structure and energy dispersive x-ray (EDX) to determine the element content. TiNT demonstrated a well-ordered structure, but the nanotubes tend to clump together upon deposition of Ag. The effect of Ag deposition on the photoelectrochemical performance of TiNT was studied where almost one-fold enhancement in the photoelectrochemical property was observed for AgTiNT compared to pure TiNT. Universiti Teknologi MARA Shah Alam 2020 Article PeerReviewed text en https://ir.uitm.edu.my/id/eprint/43485/1/43485.pdf Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /. (2020) Malaysian Journal of Chemical Engineering and Technology (MJCET) <https://ir.uitm.edu.my/view/publication/Malaysian_Journal_of_Chemical_Engineering_and_Technology_=28MJCET=29/>, 3 (2). pp. 11-17. ISSN 2682-8588
spellingShingle Carbon nanotubes. Nanoparticles. Nanostructured materials
Lim, Ying Pei
Kanakaraju, Devagi
Lim, Ying Chin
Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /
title Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /
title_full Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /
title_fullStr Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /
title_full_unstemmed Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /
title_short Photocatalytic deposition of silver particles on titania nanotube thin films: Influence of precursor concentration /
title_sort photocatalytic deposition of silver particles on titania nanotube thin films: influence of precursor concentration /
topic Carbon nanotubes. Nanoparticles. Nanostructured materials
url https://ir.uitm.edu.my/id/eprint/43485/1/43485.pdf
https://ir.uitm.edu.my/id/eprint/43485/
url_provider http://ir.uitm.edu.my/