One pot synthesis of cofe silica rice husk catalyst

With the increasing demand for sustainable catalysts, this study investigates the use of rice husk ash (RHA), a silica-rich byproduct of rice production, to develop silica supported catalysts. The problem of underutilizing agricultural waste for high-value products and the challenge of optimizing ca...

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Main Author: Azhar, Muhammad Iqbal
Format: Student Project
Language:en
Published: 2024
Subjects:
Online Access:https://ir.uitm.edu.my/id/eprint/110885/1/110885.pdf
https://ir.uitm.edu.my/id/eprint/110885/
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author Azhar, Muhammad Iqbal
author_facet Azhar, Muhammad Iqbal
author_sort Azhar, Muhammad Iqbal
building Tun Abdul Razak Library
collection Institutional Repository
content_provider Universiti Teknologi Mara
content_source UiTM Institutional Repository
continent Asia
country Malaysia
description With the increasing demand for sustainable catalysts, this study investigates the use of rice husk ash (RHA), a silica-rich byproduct of rice production, to develop silica supported catalysts. The problem of underutilizing agricultural waste for high-value products and the challenge of optimizing catalytic performance with different metal species are addressed. Monometallic cobalt (Co), monometallic iron (Fe), and bimetallic CoFe catalysts were synthesized using a one pot synthesis using sol-gel method at pH 7. Characterization using X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy-dispersive X-ray Spectroscopy (EDX), and Fourier-transform Infrared Spectroscopy (FT-IR) confirmed successful synthesis and metal incorporation. XRD identified CoFe alloy phases and amorphous silica, SEM and EDX revealed uniform metal dispersion, and FT-IR confirmed metalsilica bonding. The bimetallic CoFe catalyst showed superior catalytic performance compared to the monometallic variants, demonstrating the effectiveness of combining Co and Fe. This study highlights the potential of RHA as a sustainable silica source for catalysts and provides a foundation for further optimization in industrial applications.
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spelling my.uitm.ir-1108852025-09-30T09:07:25Z https://ir.uitm.edu.my/id/eprint/110885/ One pot synthesis of cofe silica rice husk catalyst Azhar, Muhammad Iqbal Physical and theoretical chemistry With the increasing demand for sustainable catalysts, this study investigates the use of rice husk ash (RHA), a silica-rich byproduct of rice production, to develop silica supported catalysts. The problem of underutilizing agricultural waste for high-value products and the challenge of optimizing catalytic performance with different metal species are addressed. Monometallic cobalt (Co), monometallic iron (Fe), and bimetallic CoFe catalysts were synthesized using a one pot synthesis using sol-gel method at pH 7. Characterization using X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Energy-dispersive X-ray Spectroscopy (EDX), and Fourier-transform Infrared Spectroscopy (FT-IR) confirmed successful synthesis and metal incorporation. XRD identified CoFe alloy phases and amorphous silica, SEM and EDX revealed uniform metal dispersion, and FT-IR confirmed metalsilica bonding. The bimetallic CoFe catalyst showed superior catalytic performance compared to the monometallic variants, demonstrating the effectiveness of combining Co and Fe. This study highlights the potential of RHA as a sustainable silica source for catalysts and provides a foundation for further optimization in industrial applications. 2024-08 Student Project NonPeerReviewed text en https://ir.uitm.edu.my/id/eprint/110885/1/110885.pdf Azhar, Muhammad Iqbal (2024) One pot synthesis of cofe silica rice husk catalyst. (2024) [Student Project] (Unpublished)
spellingShingle Physical and theoretical chemistry
Azhar, Muhammad Iqbal
One pot synthesis of cofe silica rice husk catalyst
title One pot synthesis of cofe silica rice husk catalyst
title_full One pot synthesis of cofe silica rice husk catalyst
title_fullStr One pot synthesis of cofe silica rice husk catalyst
title_full_unstemmed One pot synthesis of cofe silica rice husk catalyst
title_short One pot synthesis of cofe silica rice husk catalyst
title_sort one pot synthesis of cofe silica rice husk catalyst
topic Physical and theoretical chemistry
url https://ir.uitm.edu.my/id/eprint/110885/1/110885.pdf
https://ir.uitm.edu.my/id/eprint/110885/
url_provider http://ir.uitm.edu.my/