Preparation of transition metal sulfide nanoparticles via hydrothermal route
Nano sized copper sulfide, iron sulfide and molybdenum sulfide were successfully synthesised via a simple hydrothermal method. Sodium thiosulfate pentahydrate (Na2S2O3¥5H2O) and hydroxylamine sulfate ((H3NO)2¥H2SO4) were used as the starting materials and reacted with the transition metal source at...
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| Format: | Article |
| Language: | en |
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Universiti Kebangsaan Malaysia
2010
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| Online Access: | http://journalarticle.ukm.my/7326/1/01_Md_Yeaminhossain.pdf http://journalarticle.ukm.my/7326/ http://www.ukm.my/jsm/english_journals/vol39num2_2010/contentsVol39num2_2010.html |
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| author | Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang, |
| author_facet | Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang, |
| author_sort | Fei-Ling Pua, |
| building | Tun Sri Lanang Library |
| collection | Institutional Repository |
| content_provider | Universiti Kebangsaan Malaysia |
| content_source | UKM Journal Article Repository |
| continent | Asia |
| country | Malaysia |
| description | Nano sized copper sulfide, iron sulfide and molybdenum sulfide were successfully synthesised via a simple hydrothermal method. Sodium thiosulfate pentahydrate (Na2S2O3¥5H2O) and hydroxylamine sulfate ((H3NO)2¥H2SO4) were used as the starting materials and reacted with the transition metal source at 200oC for 90 min. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX) and Fourier transform infrared spectroscopy (FTIR). Spherical shape CuS and FeS2 nanoparticles with high crystallinity were successfully produced. The transmission electron micrographs revealed the well-dispersibility of the produced nanoparticles. Scanning electron micrograph showed the MoS2 nanoparticles possessed a spherical shape with sheet-like structure covering on the outer surface of the particles. |
| format | Article |
| id | my-ukm.journal-7326 |
| institution | Universiti Kebangsaan Malaysia |
| language | en |
| publishDate | 2010 |
| publisher | Universiti Kebangsaan Malaysia |
| record_format | eprints |
| spelling | my-ukm.journal-73262016-12-14T06:43:45Z http://journalarticle.ukm.my/7326/ Preparation of transition metal sulfide nanoparticles via hydrothermal route Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang, Nano sized copper sulfide, iron sulfide and molybdenum sulfide were successfully synthesised via a simple hydrothermal method. Sodium thiosulfate pentahydrate (Na2S2O3¥5H2O) and hydroxylamine sulfate ((H3NO)2¥H2SO4) were used as the starting materials and reacted with the transition metal source at 200oC for 90 min. The products were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX) and Fourier transform infrared spectroscopy (FTIR). Spherical shape CuS and FeS2 nanoparticles with high crystallinity were successfully produced. The transmission electron micrographs revealed the well-dispersibility of the produced nanoparticles. Scanning electron micrograph showed the MoS2 nanoparticles possessed a spherical shape with sheet-like structure covering on the outer surface of the particles. Universiti Kebangsaan Malaysia 2010-04 Article PeerReviewed application/pdf en http://journalarticle.ukm.my/7326/1/01_Md_Yeaminhossain.pdf Fei-Ling Pua, and Chin-Hua Chia, and Sarani Zakaria, and Tze-Khong Liew, and Mohd Ambar Yarmo, and Nay-Ming Huang, (2010) Preparation of transition metal sulfide nanoparticles via hydrothermal route. Sains Malaysiana, 39 (2). pp. 243-248. ISSN 0126-6039 http://www.ukm.my/jsm/english_journals/vol39num2_2010/contentsVol39num2_2010.html |
| spellingShingle | Fei-Ling Pua, Chin-Hua Chia, Sarani Zakaria, Tze-Khong Liew, Mohd Ambar Yarmo, Nay-Ming Huang, Preparation of transition metal sulfide nanoparticles via hydrothermal route |
| title | Preparation of transition metal sulfide nanoparticles via hydrothermal route |
| title_full | Preparation of transition metal sulfide nanoparticles via hydrothermal route |
| title_fullStr | Preparation of transition metal sulfide nanoparticles via hydrothermal route |
| title_full_unstemmed | Preparation of transition metal sulfide nanoparticles via hydrothermal route |
| title_short | Preparation of transition metal sulfide nanoparticles via hydrothermal route |
| title_sort | preparation of transition metal sulfide nanoparticles via hydrothermal route |
| url | http://journalarticle.ukm.my/7326/1/01_Md_Yeaminhossain.pdf http://journalarticle.ukm.my/7326/ http://www.ukm.my/jsm/english_journals/vol39num2_2010/contentsVol39num2_2010.html |
| url_provider | http://journalarticle.ukm.my/ |