The effect of residence time on the physical characteristics of PAN-based fibers produced using a solvent-free coagulation process

The paper reports the fabrication and characterizations of PAN fibers fabricated using residence time in the range of 2–5 s in the solvent-free coagulation process. The PAN fibers were characterized using SEM, FTIR-ATR and tensile testing. The SEM photographs revealed that the cross-section of PAN...

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主要な著者: A. Rahman, M., Ismail, A. F., Mustafa, A.
フォーマット: 論文
言語:English
出版事項: Elsevier 2007
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オンライン・アクセス:http://eprints.utm.my/id/eprint/824/2/M.A.Rahman2007_TheEffectOfResidenceTime.pdf
http://eprints.utm.my/id/eprint/824/
http://dx.doi.org/10.1016/j.msea.2006.10.042
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要約:The paper reports the fabrication and characterizations of PAN fibers fabricated using residence time in the range of 2–5 s in the solvent-free coagulation process. The PAN fibers were characterized using SEM, FTIR-ATR and tensile testing. The SEM photographs revealed that the cross-section of PAN fiber for all samples were free from large voids. A residence time of 3 s was found to be the most suitable residence time for fabricating the PAN fibers in the solvent-free coagulation bath. FTIR-ATR data suggest that the PAN fibers possessed better molecular orientation and exhibited the highest Young’s modulus of 2.55 GPa.