1-(2,3,4-Trihydroxybenzylidene)-4-ethylthiosemicarbazide

In the title molecule, C(10)H(13)N(3)O(3)S, the thiosemicarbazide =N-NH-C(=S)-NH- fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)degrees]. A weak N-H center dot center dot center dot S hydrogen bond [3.480 (1) angstrom] links two molecules about a center of inversion...

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書目詳細資料
Main Authors: Shawish, H.B., Maah, Mohd Jamil, Ng, S.W.
格式: Article
出版: International Union of Crystallography 2010
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在線閱讀:http://eprints.um.edu.my/14462/
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實物特徵
總結:In the title molecule, C(10)H(13)N(3)O(3)S, the thiosemicarbazide =N-NH-C(=S)-NH- fragment is twisted with respect to the aromatic ring [dihedral angle = 20.5 (1)degrees]. A weak N-H center dot center dot center dot S hydrogen bond [3.480 (1) angstrom] links two molecules about a center of inversion to generate a ring. The hydroxy groups are engaged in intermolecular hydrogen bonding; the O-H center dot center dot center dot O and O-H center dot center dot center dot S hydrogen bonds generate a layer motif.